2,4-己二炔-1,6-二醇合成路线 （共 39 条）
反应条件
pyrrolidine; copper(l) iodide T=0 - 20°C; 0.5 h;
参考文献
TECHNION RESEARCH and DEVELOPMENT FOUNDATION LTD.
Patent: WO2005/23816 A2, 2005 ;
Location in patent: Page/Page column 63 ;
反应条件
copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in acetonitrile T=25°C; 24 h;
参考文献
Fairlamb, Ian J. S.; Baeuerlein, Patrick S.; Marrison, Lester R.; Dickinson, Julia M.
Chemical Communications, 2003 , # 5 p. 632 - 633
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-butylamine in benzene T=45°C; Sonogashira Cross-Coupling; Inert atmosphere; Further stages;
参考文献
Tetrahedron Letters, , vol. 55, # 11 p. 1883 - 1885
反应条件
N-butylamine; copper(l) chloride; hydroxylamine hydrochloride in dichloromethane; water T=0 - 20°C;
参考文献
Journal of the American Chemical Society, , vol. 129, # 21 p. 6692 - 6693
反应条件
Cu2(OH)3OAc*H2O in acetonitrile T=100°C; 0.166667 h; Microwave irradiation;
参考文献
Chemical Communications, , vol. 46, # 13 p. 2274 - 2276
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine in toluene T=85°C; Sonogashira cross-coupling; Inert atmosphere;
参考文献
Kane, Christopher M.; Meyers, Tiffany B.; Yu, Xin; Gerken, Michael; Etzkorn, Markus
European Journal of Organic Chemistry, 2011 , # 16 p. 2969 - 2980
反应条件
copper acetylacetonate; iron (III) acetylacetonate; potassium carbonate in N,N-dimethyl-formamide T=50°C; 12 h;
参考文献
Tetrahedron, , vol. 66, # 23 p. 4029 - 4031
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine; triphenylphosphine in toluene T=85°C; Sonogashira cross-coupling; Inert atmosphere;
参考文献
Kane, Christopher M.; Meyers, Tiffany B.; Yu, Xin; Gerken, Michael; Etzkorn, Markus
European Journal of Organic Chemistry, 2011 , # 16 p. 2969 - 2980
反应条件
copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride T=60°C; Sonogashira reaction; 3 h;
参考文献
Tetrahedron, , vol. 57, # 37 p. 7871 - 7881
