2,3-二氯六氟-2-丁烯合成路线 （共 73 条）
反应条件
sodium hypochlorite in acetonitrile T=-10 - 10°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Filyakova, T. I.; Matochkina, E. G.; Peschanskii, N. V.; Kodess, M. I.; Zapevalov, A. Ya.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 1.1 p. 20 - 28
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 1 p. 25 - 35
反应条件
chlorine im UV-Licht;
参考文献
Haszeldine; Nyman
Journal of the Chemical Society, 1959 , p. 387,395
参考文献
Henne; Hinkamp; Zimmerschied
Journal of the American Chemical Society, 1945 , vol. 67, p. 1908
反应条件
hydrogen; copper on carbon T=310 - 340°C; 0.0188889 - 0.0347222 h; Product distribution / selectivity;
参考文献
E.I.du pont de Nemours and Company
Patent: US2009/12335 A1, 2009 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen; copper on calcium fluoride T=250 - 450°C; 0.0125 h; Product distribution / selectivity;
参考文献
E.I.du pont de Nemours and Company
Patent: US2009/12335 A1, 2009 ;
Location in patent: Page/Page column 6 ;
反应条件
hydrogen; palladium/barium chloride on alumina T=240 - 400°C; 0.00277778 - 0.00833333 h; Product distribution / selectivity;
参考文献
E.I.du pont de Nemours and Company
Patent: US2009/12335 A1, 2009 ;
Location in patent: Page/Page column 4-5 ;
反应条件
hydrogen; Pd-BaSO4 T=100 - 200°C; 0.0166667 h; Product distribution / selectivity;
参考文献
E.I.du pont de Nemours and Company
Patent: US2009/12335 A1, 2009 ;
Location in patent: Page/Page column 4 ;
反应条件
hydrogen; palladium on calcium fluoride poisoned with lead acetate T=200 - 300°C; 0.000694444 - 0.00833333 h; Product distribution / selectivity;
参考文献
E.I.du pont de Nemours and Company
Patent: US2009/12335 A1, 2009 ;
Location in patent: Page/Page column 8 ;
反应条件
hydrogen T=240°C; 4 h; optical yield given as percent de;
参考文献
Stepanov; Delyagina; Cherstkov
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 9 p. 1290 - 1295
参考文献
Henne et al.
Journal of the American Chemical Society, 1947 , vol. 69, p. 1819
