1-(5-乙酰基-2-羟基-苯基)-乙酮合成路线 （共 18 条）
反应条件
acetic anhydride; triethylamine 16 h; Heating;
参考文献
Sangwan; Verma; Malik; Dhindsa
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 3 p. 294 - 296
反应条件
potassium hydroxide in methanol
参考文献
Singh, O. V.; Sangeeta; Khanna, M. S.; Garg, C. P.; Kapoor, R. P.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 12 p. 1241 - 1248
反应条件
1: aq.-ethanolic NaOH 2: aq.-ethanolic NaOH View Scheme
参考文献
Limaye; Pendse
Rasayanam, 1956 , vol. 2, p. 124,130
反应条件
aluminium trichloride
T=150°C; 3 h;
参考文献
Sangwan, Naresh K.; Verma, Braham S.; Dhindsa, Kuldip Singh
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 672 - 674
反应条件
thionyl chloride in acetonitrile
T=29.84°C; Kinetics; TemperatureReagent/catalyst;
参考文献
Venkateswarlu, Marri; Satish Kumar, Mukka; Ramgopal, Soma; Rajanna, Kamatala Chinna; Umesh Kumar, Utkoor; Uppalaiah, Kusampally; Saiprakash, Pondichery Kuppuswamy
Helvetica Chimica Acta, 2011 , vol. 94, # 12 p. 2168 - 2187
反应条件
aluminium trichloride in carbon disulfide
1 h; Heating;
参考文献
Singh, O. V.; Sangeeta; Khanna, M. S.; Garg, C. P.; Kapoor, R. P.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 12 p. 1241 - 1248
反应条件
aluminium trichloride in 1,2-dichloro-ethane
T=50°C; 30 h; Further byproducts given;
参考文献
Fedenok, L. G.; Myasnikova, R. N.; Shvartsberg, M. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 8 p. 1685 - 1688
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 8 p. 1836 - 1839
反应条件
1: 88 percent / NaOH / TBAH / CH2Cl2 / 1.5 h / Ambient temperature
2: 1) 60percent AlCl3 / 3 h / 150 °C
View Scheme
参考文献
Henning, H.-G.; Schwabe, B.; Kernchen, F.; Westphal, G.
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 3 p. 491 - 501
反应条件
in hexane
6 h; Irradiation;
参考文献
Garcia, Hermenegildo; Martinez-Utrilla, Roberto; Miranda, Miguel A.
Tetrahedron, 1985 , vol. 41, # 15 p. 3131 - 3134
反应条件
1: sulfuryl dichloride; silica gel / neat (no solvent) / 20 °C / |Microwave irradiation
2: sulfuryl dichloride; silica gel / neat (no solvent) / 20 °C / |Microwave irradiation
View Scheme
参考文献
Satish Kumar, Mukka; Chinna Rajanna, Kamatala; Venkanna, Purugula; Venkateswarlu, Marri
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1756 - 1759
