4,4',4'-三氯三苯甲基乙醇合成路线 (共 10 条)
参考文献
Journal of the American Chemical Society, , vol. 73, p. 3644,3645
参考文献
Journal of the American Chemical Society, , vol. 79, p. 579
反应条件
1: 1-chloro-4-bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: chloroformic acid ethyl ester in tetrahydrofuran; hexane T=-78°C; 3 h; 3: With ammonium chloride in tetrahydrofuran; hexane; water
参考文献
Tetrahedron, , vol. 68, # 24 p. 4701 - 4709
反应条件
trifluoroacetic acid; dibenzoyl peroxide in 1,2-dichloro-ethane T=50°C; 24 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1987 - 1996
反应条件
in tetrahydrofuran 0.833333 h; Heating;
参考文献
Journal of Physical Organic Chemistry, , vol. 10, # 7 p. 499 - 513
反应条件
in tetrahydrofuran Heating;
参考文献
Canadian Journal of Chemistry, , vol. 64, p. 1758 - 1763
参考文献
Chemische Berichte, , vol. 38, p. 337
反应条件
CF3CO3H; trifluoroacetic acid in 1,2,2-trifluoro-trichloroethane T=-25°C; Criegee rearrangement; 1 h;
参考文献
Krasutsky, Pavel A.; Kolomitsyn, Igor V.; Krasutsky, Sergiy G.; Kiprof, Paul
Organic Letters, 2004 , vol. 6, # 15 p. 2539 - 2542
反应条件
zinc(II) chloride in acetic acid Heating;
参考文献
Schorr,M.
Justus Liebigs Annalen der Chemie, 1963 , vol. 661, p. 157 - 164
反应条件
formic acid in acetic acid
14 h; Heating;
参考文献
Andrews, Adrian F.; Mackie, Raymond K.; Walton, John C.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 96 - 102