in tetrahydrofuran Ar atmosphere, RYbI transferring dropwise under Ar pressure at room temperature, 2 to 3 h, Me3SnCl addn.; extracting with ether, extracts drying (Na2SO4);
参考文献
Russian Journal of General Chemistry, , vol. 67, # 1 p. 76 - 78
Morgan; Drew
Journal of the Chemical Society, 1925 , vol. 127, p. 1760,1763,1765
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Kraus, C. A.; Forster, L. S.
Journal of the American Chemical Society, 1927 , vol. 49, p. 457 - 467
in ethylene glycol dimethyl ether Electrolysis; (N2); potential controlled electrolysis at -2,0 V (vs. AgI/Ag referenceelectrode) of soln. of Ge compd. at room temp.; filtered soln. was evapd. in vac., residue was extd. with ether and solvent removed, residue was sepd. by TLC, products were identified by m. p., IR, NMR and MAS;
参考文献
Corriu, R. J. P.; Dabosi, G.; Martineau, M.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 63 - 72
phenol in ethylene glycol dimethyl ether Electrolysis; (N2); potential controlled electrolysis at -2,0 V (vs. AgI/Ag referenceelectrode) of soln. of Ge compd. at room temp. in presence of PhOH/PhOD; filtered soln. was evapd. in vac., residue was extd. with ether and solvent removed, residue was sepd. by TLC, products were identified by m. p., IR, NMR and MAS;
参考文献
Corriu, R. J. P.; Dabosi, G.; Martineau, M.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 63 - 72
in ethylene glycol dimethyl ether Electrolysis; (N2); potential controlled electrolysis at -1,3 V (vs. AgI/Ag referenceelectrode) of soln. of Ge compd. at room temp. in presence of Me3SiCl; filtered soln. was evapd. in vac., residue was extd. with ether and solvent removed, residue was sepd. by TLC, products were identified by m. p., IR, NMR and MAS;
参考文献
Corriu, R. J. P.; Dabosi, G.; Martineau, M.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 63 - 72
in ethylene glycol dimethyl ether Electrolysis; (N2); potential controlled electrolysis at -1,6 V (vs. AgI/Ag referenceelectrode) of soln. of Ge compd. at room temp. in presence of Me3SiCl; filtered soln. was evapd. in vac., residue was extd. with ether and solvent removed, residue was sepd. by TLC, products were identified by m. p., IR, NMR and MAS;
参考文献
Corriu, R. J. P.; Dabosi, G.; Martineau, M.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 63 - 72
in ethylene glycol dimethyl ether Electrolysis; (N2); potential controlled electrolysis at -2,0 V (vs. AgI/Ag referenceelectrode) of soln. of Ge compd. at room temp.; filtered soln. was evapd. in vac., residue was extd. with ether and solvent removed, residue was sepd. by TLC, products were identified by m. p., IR, NMR and MAS;
参考文献
Corriu, R. J. P.; Dabosi, G.; Martineau, M.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 63 - 72
Johnson; Nebergall
Journal of the American Chemical Society, 1949 , vol. 71, p. 1721
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Johnson; Nebergall; Harris
Inorganic Syntheses, 1957 , vol. 5, p. 76
phenol in ethylene glycol dimethyl ether Electrolysis; (N2); potential controlled electrolysis at -2,0 V (vs. AgI/Ag referenceelectrode) of soln. of Ge compd. at room temp. in presence of PhOH/PhOD; filtered soln. was evapd. in vac., residue was extd. with ether and solvent removed, residue was sepd. by TLC, products were identified by m. p., IR, NMR and MAS;
参考文献
Corriu, R. J. P.; Dabosi, G.; Martineau, M.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 63 - 72
