DL-1,4-二溴-2,3-二丁醇合成路线 （共 9 条）
反应条件
acetyl-bromide in 1,4-dioxane T=20°C;
参考文献
Halila, Sami; Benazza, Mohammed; Demailly, Gilles
Tetrahedron Letters, 2001 , vol. 42, # 19 p. 3307 - 3310
反应条件
osmium(VIII) oxide; dihydrogen peroxide in tert-butyl alcohol
参考文献
Torf,S.F.; Khromov-Borisov,N.V.
J. Gen. Chem. USSR (Engl. Transl.), 1962 , vol. 32, p. 1838 - 1846,1822 - 1828
反应条件
potassium permanganate; water; magnesium sulfate T=-2 - 0°C;
参考文献
Griner
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1893 , vol. 117, p. 554
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Thiele
Justus Liebigs Annalen der Chemie, 1899 , vol. 308, p. 339
反应条件
tetrahydrofuran; water; hydrogen bromide
参考文献
Bose et al.
Journal of the Chemical Society, 1959 , p. 3314,3319
反应条件
dianhydride of inactive cleavable erythritol;
参考文献
Griner
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1893 , vol. 117, p. 554
参考文献
Justus Liebigs Annalen der Chemie, , vol. 308, p. 339
反应条件
N-ethyl-N,N-diisopropylamine; (9S)-6'-methoxycinchonan-9-yl diphenylphosphinite in various solvent(s) T=-78°C; 1 h; Title compound not separated from byproducts;
参考文献
Mizuta, Shinya; Ohtsubo, Yutaka; Tsuzuki, Takeo; Fujimoto, Tetsuya; Yamamoto, Iwao
Tetrahedron Letters, 2006 , vol. 47, # 47 p. 8227 - 8229
反应条件
N-ethyl-N,N-diisopropylamine; (9S)-6'-methoxycinchonan-9-yl diphenylphosphinite in various solvent(s) T=-78°C; 1 h; Title compound not separated from byproducts;
参考文献
Mizuta, Shinya; Ohtsubo, Yutaka; Tsuzuki, Takeo; Fujimoto, Tetsuya; Yamamoto, Iwao
Tetrahedron Letters, 2006 , vol. 47, # 47 p. 8227 - 8229
反应条件
T=25°C; zeitlicher Verlauf;
参考文献
Bose et al.
Journal of the Chemical Society, 1959 , p. 3314,3319
