3,5-二溴-4-羟基苯甲醛合成路线 （共 27 条）
反应条件
oxygen; [Co(O2CCH3)2]*4H2O; sodium hydroxide in ethylene glycol T=80°C; P=760.051 Torr; 8 h; Reagent/catalystTemperature;
参考文献
Jiang, Jian-An; Chen, Cheng; Guo, Ying; Liao, Dao-Hua; Pan, Xian-Dao; Ji, Ya-Fei
Green Chemistry, 2014 , vol. 16, # 5 p. 2807 - 2814
参考文献
Kumar, Lalit; Mahajan, Tanu; Agarwal
Green Chemistry, 2011 , vol. 13, # 8 p. 2187 - 2196
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; copper diacetate in water; acetonitrile T=20°C; 4 h; Green chemistry;
参考文献
Jiang, Jian-An; Du, Jia-Lei; Wang, Zhan-Guo; Zhang, Zhong-Nan; Xu, Xi; Zheng, Gan-Lin; Ji, Ya-Fei
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1677 - 1681
反应条件
oxygen; [Co(O2CCH3)2]*4H2O; sodium hydroxide T=80°C; P=760.051 Torr; 4 h;
参考文献
Tetrahedron Letters, , vol. 55, # 8 p. 1406 - 1411
反应条件
hexamethylenetetramine-bromine complex; silica gel in dichloromethane T=20°C; 0.0833333 h;
参考文献
Tetrahedron Letters, , vol. 46, # 51 p. 8959 - 8963
反应条件
hydrogenchloride in methanol T=5°C; 4.5 h; Yield given;
参考文献
Synthetic Communications, , vol. 20, # 17 p. 2659 - 2666
反应条件
Fremy’s salt in chloroform 18 h; pH 6;
参考文献
Saa, Jose M.; Morey, Jeronimo; Rubido, Carmen
Journal of Organic Chemistry, 1986 , vol. 51, # 23 p. 4471 - 4473
反应条件
hydrogenchloride; bromine 1.) chlorobenzene, reflux, 4 h, 2.) MeOH; Yield given. Multistep reaction;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 32, # 8 p. 872 - 873
反应条件
1: AlCl3, aluminium chloride / dichloromethane 2: bromine; acetic acid View Scheme
参考文献
Letters in Drug Design and Discovery, , vol. 9, # 6 p. 604 - 610
反应条件
water in 1,4-dioxane T=34°C; Kinetics;
参考文献
Tetrahedron Letters, , vol. 23, # 12 p. 1305 - 1308
