Titanium(IV) oxide; trifluoroacetic acid in acetonitrile 24 h; Ambient temperatureIrradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lai; Mallouk
Journal of the Chemical Society - Series Chemical Communications, 1993 , # 17 p. 1359 - 1361
Titanium(IV) oxide; trifluoroacetic acid in acetonitrile 24 h; Ambient temperatureIrradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lai; Mallouk
Journal of the Chemical Society - Series Chemical Communications, 1993 , # 17 p. 1359 - 1361
Titanium(IV) oxide; trifluoroacetic acid in acetonitrile 24 h; Ambient temperatureIrradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lai; Mallouk
Journal of the Chemical Society - Series Chemical Communications, 1993 , # 17 p. 1359 - 1361
Titanium(IV) oxide; trifluoroacetic acid in acetonitrile 24 h; Ambient temperatureIrradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lai; Mallouk
Journal of the Chemical Society - Series Chemical Communications, 1993 , # 17 p. 1359 - 1361
Peterson,L.K.; Burg,A.B.
Journal of the American Chemical Society, 1964 , vol. 86, p. 2587 - 2591
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Gmelin Handbook: F: PerFHalOrg.3, 1.4, page 31 - 40
in neat (no solvent) Cl2S=NTeF5 and CF3COOAg stirred at room temp. and warmed to 45°Cand stirred for 1 h; O=S=NTeF5 and (CF3CO)2O condensed into -196°C trap under vac., separation achieved by trap-to-trap distillation through -45 (O=S=NTeF5) and -78°C cooled traps; elem. anal.;
参考文献
Hartl, Hans; Huppmann, Peter; Lentz, Dieter; Seppelt, Konrad
Inorganic Chemistry, 1983 , vol. 22, p. 2183 - 2187
byproducts: AgI; below 20°C; further react. in equil.; distn.; main product as medium fraction at 0°C / 55 Torr;
参考文献
Peterson,L.K.; Burg,A.B.
Journal of the American Chemical Society, 1964 , vol. 86, p. 2587 - 2591
Full Text View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.3, 1.4, page 31 - 40