反应条件
1.1: NaHMDS / tetrahydrofuran / 1.5 h / 18 °C
1.2: 30 percent / tetrahydrofuran / 15 h / 18 °C
2.1: 57 percent / LiAlH4 / diethyl ether / 1.5 h
3.1: 70 percent / NaH; NaI / dimethylformamide / 18 h / 18 °C
4.1: Rh2(OAc)4 / CH2Cl2 / 0.5 h / 18 °C
5.1: 210 mg / H2 / 5percent Pd/C / CH2Cl2; ethyl acetate; ethanol / 22 h / 18 °C / 760.05 Torr
View Scheme
参考文献
Banwell, Martin G.; Edwards, Alison J.; Jolliffe, Katrina A.; Smith, Jason A.; Hamel, Ernest; Verdier-Pinard, Pascal
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 2 p. 296 - 305
