N-乙酰基-3,5-二硝基-L-酪氨酸乙酯合成路线 （共 9 条）
反应条件
thionyl chloride; benzene Erwaermen des Reaktionsprodukts mit Aethanol;
参考文献
Bruice et al.
Journal of Organic Chemistry, 1953 , vol. 18, p. 83,87
反应条件
1: acetic acid; concentrated H2SO4; concentrated aqueous HNO3 2: SOCl2; benzene / Erwaermen des Reaktionsprodukts mit Aethanol View Scheme
参考文献
Bruice et al.
Journal of Organic Chemistry, 1953 , vol. 18, p. 83,87
反应条件
1: aq. NaOH solution 2: toluene-sulfonic acid-(4) View Scheme
参考文献
Chalmers et al.
Journal of the Chemical Society, 1949 , p. 3424,3432
反应条件
1: HNO3+H2SO4 2: aq. NaOH solution 3: toluene-sulfonic acid-(4) View Scheme
参考文献
Chalmers et al.
Journal of the Chemical Society, 1949 , p. 3424,3432
反应条件
toluene-4-sulfonic acid
参考文献
Chalmers et al.
Journal of the Chemical Society, 1949 , p. 3424,3432
反应条件
(i) (nitration), (ii) /BRN= 1718733/, /BRN= 605303/; Multistep reaction;
参考文献
Buess,C.M. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 469 - 474
反应条件
1: toluene-sulfonyl chloride-(4); pyridine / anschliessendes Erhitzen mit 4-Methoxy-phenol 2: palladium; methanol / Hydrogenation View Scheme
参考文献
Chalmers et al.
Journal of the Chemical Society, 1949 , p. 3424,3432
反应条件
1: toluene-sulfonyl chloride-(4); pyridine / anschliessendes Erhitzen mit 4-Methoxy-phenol 2: palladium; methanol / Hydrogenation 3: Diazotization View Scheme
参考文献
Chalmers et al.
Journal of the Chemical Society, 1949 , p. 3424,3432
反应条件
1: MeSO2Cl
2: (i) (catalytic hydrogenation), (ii) NaNO2, H2SO4, (iii) aq. NaI, I2, CHCl3, urea
3: aq. HCl / acetic acid
View Scheme
参考文献
Buess,C.M. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 469 - 474
