4-(二甲基氨基)苯甲醛缩氨基硫脲合成路线 （共 10 条）
反应条件
in ethanol; water Reflux;
参考文献
Alam, Mohammad Sayed; Liu, Lijun; Lee, Yong-Eok; Lee, Dong-Ung
Chemical and Pharmaceutical Bulletin, 2011 , vol. 59, # 5 p. 568 - 573
Title/Abstract Full Text View citing articles Show Details
Alam, Mohammad Sayed; Liu, Lijun; Lee, Dong Ung
Chemical and Pharmaceutical Bulletin, 2011 , vol. 59, # 11 p. 1413 - 1416
反应条件
sodium acetate in water T=20°C;
参考文献
Rajak, Harish; Agarawal, Avantika; Parmar, Poonam; Thakur, Bhupendra Singh; Veerasamy, Ravichandran; Sharma, Prabodh Chander; Kharya, Murli Dhar
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 19 p. 5735 - 5738
反应条件
1: 1 h / 140 °C 2: 1.) NaNO2, HCl / 1.) glacial CH3COOH, 2.) pyridine, room temp., overnight View Scheme
参考文献
Pande; Kalsi; Bhalla; Barthwal
Pharmazie, 1987 , vol. 42, # 4 p. 269 - 269
反应条件
1: 1 h / 140 °C 2: 1.) NaNO2, HCl / 1.) glacial CH3COOH, 2.) pyridine, room temp., overnight View Scheme
参考文献
Pande; Kalsi; Bhalla; Barthwal
Pharmazie, 1987 , vol. 42, # 4 p. 269 - 269
反应条件
hexaaquairon(III) perchlorate 2 h;
参考文献
Parmar, Anupama; Goyal, Rita; Kumar, Baldev; Kumar, Harish
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1998 , vol. 37, # 9 p. 941 - 942
反应条件
pyridine; hydrogenchloride; sodium nitrite 1) glacial acetic acid, water, 0-5 deg C, 2) room temperature, overnight; Multistep reaction;
参考文献
Srivastava; Palit; Singh; Dhawan; Shanker
Journal of the Indian Chemical Society, 1990 , vol. 67, # 4 p. 335 - 338
反应条件
anhydrous iron chloride; sodium acetate in acetic acid T=20°C; 0.5 h;
参考文献
Rajak, Harish; Agarawal, Avantika; Parmar, Poonam; Thakur, Bhupendra Singh; Veerasamy, Ravichandran; Sharma, Prabodh Chander; Kharya, Murli Dhar
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 19 p. 5735 - 5738
反应条件
1: 1 h / 140 °C
2: 1.) NaNO2, HCl / 1.) glacial CH3COOH, 2.) pyridine, room temp., overnight
View Scheme
参考文献
Pande; Kalsi; Bhalla; Barthwal
Pharmazie, 1987 , vol. 42, # 4 p. 269 - 269
反应条件
1: silica gel / dichloromethane / Microwave irradiation
2: silica gel / dichloromethane / Microwave irradiation
View Scheme
参考文献
Chattopadhyay, Gautam; Ray, Partha Sinha
Synthetic Communications, 2011 , vol. 41, # 17 p. 2607 - 2614
反应条件
silica gel in dichloromethane
Microwave irradiation;
参考文献
Chattopadhyay, Gautam; Ray, Partha Sinha
Synthetic Communications, 2011 , vol. 41, # 17 p. 2607 - 2614
