2-溴-N-甲基-N-乙酰苯胺合成路线 （共 9 条）
反应条件
triethylamine in ethyl acetate T=0 - 25°C; 0.5 h;
参考文献
Dainippon Sumitomo Pharma Co., Ltd.
Patent: EP1719761 A1, 2006 ;
Location in patent: Page/Page column 33 ;
反应条件
acetic acid T=20°C; 2 h;
参考文献
Briard, Emmanuelle; Pike, Victor W.
Journal of Labelled Compounds and Radiopharmaceuticals, 2004 , vol. 47, # 4 p. 217 - 232
参考文献
ASTRAZENECA AB; ARGENTA DISCOVERY LIMITED
Patent: WO2009/138707 A1, 2009 ;
Location in patent: Page/Page column 88-89 ;
WO 2009/138707 A1
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran T=0°C; 1 h;
参考文献
Ronsisvalle; Marrazzo; Prezzavento; Pasquinucci; Vittorio; Pittala; Pappalardo; Cacciaguerra; Spampinato
Journal of medicinal chemistry, 1998 , vol. 41, # 10 p. 1574 - 1580
参考文献
Rhone-Poulenc Rorer S.A.
Patent: US5475106 A1, 1995 ;
参考文献
Bischoff; Pessis
Chemische Berichte, 1901 , vol. 34, p. 2125
反应条件
S4N4*SbCl5 in toluene Heating;
参考文献
Kim, Kil-Joong; Kim, Kyongtae
Tetrahedron Letters, 1997 , vol. 38, # 24 p. 4227 - 4230
反应条件
Multistep reaction.;
参考文献
McAllister, Laura A.; Brand, Stephen; De Gentile, Remy; Procter, David J.
Chemical Communications, 2003 , # 18 p. 2380 - 2381
反应条件
in dimethyl sulfoxide
T=25°C; Kinetics;
参考文献
Adhikary, Keshab Kumar; Lee, Hai Whang
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 3 p. 857 - 862
