3,7-二甲基-6-辛烯-1-炔基-3-醇合成路线 （共 58 条）
参考文献
Ruzicka; Fornasir
Helvetica Chimica Acta, 1919 , vol. 2, p. 184
反应条件
1: palladium/calcium carbonate / Hydrogenation 2: hydrogen bromide / Behandeln des erhaltenen Bromids mit Kaliumacetat in Dimethylformamid und Erwaermen des Reaktionsprodukts mit wss.Natronlauge View Scheme
参考文献
Nasarow; Kamernizkii; Achrem
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 1458,1459
J. Gen. Chem. USSR (Engl. Transl.), 1958 , vol. 28, p. 1511,1512
反应条件
1: phosphoric acid 2: Lindlar-catalyst; quinoline; hexane / Hydrogenation View Scheme
参考文献
Hoffmann-La Roche
Patent: US2797235 , 1954 ;
反应条件
1: palladium/calcium carbonate / Hydrogenation 2: hydrogen bromide / Behandeln des erhaltenen Bromids mit Kaliumacetat in Dimethylformamid und Erwaermen des Reaktionsprodukts mit wss.Natronlauge View Scheme
参考文献
Nasarow; Kamernizkii; Achrem
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 1458,1459
J. Gen. Chem. USSR (Engl. Transl.), 1958 , vol. 28, p. 1511,1512
反应条件
1: NaBr / acetonitrile; H2O / 9 h / Ambient temperature; electrolysis 2: NaOH / acetonitrile; H2O / 1 h / Ambient temperature 3: 92 percent / H2(g), quinoline / 5percent Pd/BaSO4 / methanol / Ambient temperature View Scheme
参考文献
Uneyama, Kenji; Date, Takasi; Torii, Sigeru
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3160 - 3163
反应条件
1: palladium/calcium carbonate / Hydrogenation 2: aluminium tert-butylate 3: liquid ammonia; diethyl ether / ueber mehrere Stufen View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 28, p. 1458,1459
J. Gen. Chem. USSR (Engl. Transl.), , vol. 28, p. 1511,1512
反应条件
1: acetic acid anhydride; phosphoric acid 2: quinoline; petroleum ether; Lindlar-catalyst / Hydrogenation View Scheme
参考文献
Hoffmann-La Roche
Patent: US2797235 , 1954 ;
反应条件
1: phosphoric acid 2: Lindlar-catalyst; hexane / Hydrogenation View Scheme
参考文献
Hoffmann-La Roche
Patent: US2797235 , 1954 ;
反应条件
1: NaBr / acetonitrile; H2O / 9 h / Ambient temperature; electrolysis 2: NaOH / acetonitrile; H2O / 1 h / Ambient temperature 3: 92 percent / H2(g), quinoline / 5percent Pd/BaSO4 / methanol / Ambient temperature 4: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min 5: tetrahydrofuran / 0.33 h 6: 200 °C View Scheme
参考文献
Uneyama, Kenji; Date, Takasi; Torii, Sigeru
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3160 - 3163
反应条件
toluene-4-sulfonic acid
参考文献
Hoffmann-La Roche
Patent: US2861109 , 1956 ;
