3,7-二甲基-6-辛烯-1-炔基-3-醇合成路线 （共 58 条）
反应条件
succinic acid; Ph2Si(OH)2; polyvanadioorganosiloxane in xylene T=146 - 148°C; 3.5 h;
参考文献
Erman, M. B.; Aul'chenko, I. S.; Kheifits, L. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , p. 21 - 28
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 1 p. 23 - 31
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine T=20°C; 3 h;
参考文献
Fuerstner, Alois; Hannen, Peter
Chemistry - A European Journal, 2006 , vol. 12, # 11 p. 3006 - 3019
反应条件
1: aqueous phosphoric acid 2: Lindlar-catalyst; quinoline; hexane / Hydrogenation View Scheme
参考文献
Hoffmann-La Roche
Patent: US2797235 , 1954 ;
反应条件
potassium hydroxide in water T=93°C; 6.41667 h; Heating / reflux;
参考文献
EP1852410 A1, ;
Page/Page column 6 ;
反应条件
potassium hydroxide in dimethyl sulfoxide T=50°C; 6 h;
参考文献
Bulletin de la Societe Chimique de France, , # 6 p. 1250 - 1260
反应条件
potassium hydroxide in neat (no solvent) T=75 - 120°C; 0.366667 h;
参考文献
Tetrahedron Letters, , vol. 24, # 1 p. 61 - 64
反应条件
hydrogen; modified (Zn(CH3COO)2+pyridine+KOH) ShPAK-0.5 (0.5percent Pd/Al2O3) in methanol T=55°C; p(H2)=0.04 MPa;
参考文献
Tolkacheva; Kislyi; Taits; Semenov
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 2 p. 150 - 152
反应条件
hydrogen; PdAu in polystyrene-block-poly-4-vinylpyridine micelles in toluene T=90°C; P=760 Torr; 0.316667 h;
参考文献
Bronstein, Lyudmila M.; Chernyshov, Dmitrii M.; Volkov, Ilya O.; Ezernitskaya, Marina G.; Valetsky, Peter M.; Matveeva, Valentina G.; Sulman, Esther M.
Journal of Catalysis, 2000 , vol. 196, # 2 p. 302 - 314
反应条件
hydrogen; Lindlar's catalyst in octane T=20°C; P=760 Torr; other solvents (ethanol, acetic acid), other catalyst (2.8percent Pd/C); dependence of reaction rate; Product distribution;
参考文献
Demir, Mustafa M.; Gulgun, Mehmet A.; Menceloglu, Yusuf Z.; Erman, Burak; Abramchuk, Sergei S.; Makhaeva, Elena E.; Khokhlov, Alexei R.; Matveeva, Valentina G.; Sulman, Mikhail G.
Macromolecules, 2004 , vol. 37, # 5 p. 1787 - 1792
反应条件
hydrogen; modified (Zn(CH3COO)2+pyridine+KOH) ShPAK-0.5 (0.5percent Pd/Al2O3) in methanol T=55°C; p(H2)=0.04 MPa;
参考文献
Tolkacheva; Kislyi; Taits; Semenov
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 2 p. 150 - 152
