[1,1'-联环己基]-1-醇合成路线 (共 21 条)
参考文献
Zelinsky; Schuikin; Fatejew
Zhurnal Obshchei Khimii, 1932 , vol. 2, p. 671,680
Chem. Zentralbl., 1933 , vol. 104, # II p. 1673
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Signaigo; Cramer
Journal of the American Chemical Society, 1933 , vol. 55, p. 3326,3330
反应条件
in diethyl ether 0.5 h; Heating;
参考文献
Rao, R. R.; Bhattacharya, S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 3 p. 207 - 209
反应条件
1: HCOONa / methanol; H2O 2: 1) MeLi, 2) HOAc, ethanethiol / 1) THF, -40 deg C to -25 deg C, 2) THF, -25 deg C to 20 deg C View Scheme
参考文献
Baldwin, Jack E.; Adlington, Robert M.; Bottaro, Jeffrey C.; Kolhe, Jayant N.; Newington, Ian M.; Perry, Matthew W. D.
Tetrahedron, 1986 , vol. 42, # 15 p. 4235 - 4246
参考文献
Chirko,A.I.
Zhurnal Organicheskoi Khimii, 1965 , vol. 1, # 6 p. 1004 - 1007,1012 - 1014
参考文献
Wu, Tse-Chong; Xiong, Heping; Rieke, R. D.
Journal of Organic Chemistry, 1990 , vol. 55, # 17 p. 5045 - 5051
反应条件
(i) B2H6, (ii) Br2, (iii) H2O, (iv) (oxidation); Multistep reaction;
参考文献
Lane,C.F.; Brown,H.C.
Journal of the American Chemical Society, 1971 , vol. 93, p. 1025 - 1027
反应条件
(i) LiAlH4, octane, THF, (ii) /BRN= 3587209/, ethane-1,2-diol, (iii) aq. H2O2, aq. NaOH, aq. EtOH; Multistep reaction;
参考文献
Brown,H.C. et al.
Journal of the American Chemical Society, 1970 , vol. 92, p. 6648 - 6649
反应条件
Yield given. Multistep reaction;
参考文献
Baldwin, Jack E.; Bottaro, Jeffrey C.; Kolhe, Jayant N.; Adlington, Robert M.
Journal of the Chemical Society, Chemical Communications, 1984 , # 1 p. 22 - 23
反应条件
acetic acid; sodium nitrite anschliessendes Erwaermen auf 60grad;
参考文献
Tchoubar
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 228, p. 580
反应条件
1: rose-bengal; methanol; oxygen / Irradiation.UV-Licht 2: triphenylphosphine; diethyl ether 3: platinum; acetic acid; methanol / 73550.8 Torr / Hydrogenation View Scheme
参考文献
Schenck; Schulte-Elte
Justus Liebigs Annalen der Chemie, 1958 , vol. 618, p. 185,191