N-乙酰-DL-苯丙氨酸合成路线 （共 69 条）
反应条件
in methanol 6 h; Reflux;
参考文献
Naturale, Guillaume; Lamblin, Marc; Commandeur, Claude; Dessolin, Jean; Felpin, Francois-Xavier
European Journal of Organic Chemistry, 2012 , # 29 p. 5774 - 5788,15
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Naturale, Guillaume; Lamblin, Marc; Commandeur, Claude; Felpin, Francois-Xavier; Dessolin, Jean
European Journal of Organic Chemistry, 2012 , # 29 p. 5774 - 5788
反应条件
hydrogen; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in methanol; toluene P=15001.2 Torr; 16 h; Ambient temperaturevar. of ligand, pressure, asymmetric induction; Product distribution;
参考文献
Lisichkina, I. N.; Vinogradova, A. I.; Saporovskaya, M. B.; Latov, V. K.; Velikov, V. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 5 p. 1029 - 1031
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 5 p. 1170 - 1172
反应条件
hydrogen; Pd-BaSO4 in water; acetic acid T=60°C; P=2585.7 Torr; 8 h; Yields of byproduct given;
参考文献
Tou, Jacob S.; Vineyard, Billy D.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1135 - 1136
反应条件
hydrogen; titanium(IV) isopropylate; dicobalt octacarbonyl in 1,4-dioxane T=120°C; P=100 Torr; 2 h;
参考文献
Hirai, Kenji; Fujita, Makoto; Fuchikami, Takamasa
Journal of Organometallic Chemistry, 1985 , vol. 279, p. 203 - 214
反应条件
formaldehyd; palladium dichloride in sodium hydroxide T=65°C; Hydrogenation;
参考文献
Arterburn; Pannala; Gonzalez; Chamberlin
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7847 - 7849
反应条件
hydrogenchloride; sodium hydroxide in water; hydrogen
参考文献
Mitsui Toatsu Chemicals, Incorporated
Patent: US4612388 A1, 1986 ;
反应条件
dicobalt octacarbonyl; hydrogen; 1,2-bis-(diphenylphosphino)ethane in ethyl acetate T=80°C; P=108601 - 112480 Torr; 4 h;
参考文献
Lin, J.J.; Knifton, John F.
Journal of Organometallic Chemistry, 1991 , vol. 417, # 1/2 p. 99 - 110
反应条件
hydrogenchloride; sodium hydroxide in 1,4-dioxane; water
参考文献
Mitsui Toatsu Chemicals, Incorporated
Patent: US4675439 A1, 1987 ;
反应条件
formaldehyd; palladium dichloride in sodium hydroxide T=65°C; Hydrogenation;
参考文献
Arterburn; Pannala; Gonzalez; Chamberlin
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7847 - 7849
反应条件
1-methyl-pyrrolidin-2-one; sulfuric acid; lithium bromide; [PdBr2(PPh3)2] in water T=120°C; P=45003.6 Torr;
参考文献
Freed, Dana A.; Kozlowski, Marisa C.
Tetrahedron Letters, 2001 , vol. 42, # 20 p. 3403 - 3406
