3,4-二氯-3-环丁烯-1,2-二酮合成路线 （共 26 条）
反应条件
thionyl chloride; N,N-dimethyl-formamide in benzene T=80°C; 6 h;
参考文献
Malicka, Joanna M.; Sandeep, Anjamkudy; Monti, Filippo; Bandini, Elisa; Gazzano, Massimo; Ranjith, Choorikkat; Praveen, Vakayil K.; Ajayaghosh, Ayyappanpillai; Armaroli, Nicola
Chemistry - A European Journal, 2013 , vol. 19, # 39 p. 12991 - 13001
反应条件
in dichloromethane; N,N-dimethyl-formamide
参考文献
McCleland, Brent; Palovich, Michael R.; Widdowson, Katherine L.
Patent: US2004/48897 A1, 2004 ;
US 20040048897 A1
反应条件
sulfuric acid; sulfur trioxide
参考文献
Maahs,G.
Justus Liebigs Annalen der Chemie, 1965 , vol. 686, p. 55 - 63
反应条件
1: in benzene 8 h; Reflux; 2: With hydrogenchloride; acetic acid in water T=120°C; 4 h;
参考文献
Shafeekh; Rahim; Basheer; Suresh; Das
Dyes and Pigments, 2013 , vol. 96, # 3 p. 714 - 721
反应条件
in dichloromethane T=120°C; Friedel-Crafts reaction; 0.166667 h; microwave irradiation;
参考文献
Organic Letters, , vol. 6, # 1 p. 83 - 86
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rubin, Yves; Knobler, Carolyn B.; Diederich, Francois
Journal of the American Chemical Society, 1990 , vol. 112, # 4 p. 1607 - 1617
反应条件
triethylamine in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Zinner; Grunefeld
Archiv der Pharmazie, 1985 , vol. 318, # 11 p. 977 - 983
反应条件
1: in benzene 15 h; Inert atmosphereReflux; 2: With hydrogenchloride; water; acetic acid in benzene 3 h; Inert atmosphereReflux;
参考文献
Wang, Weida; Fu, Afu; You, Jingsong; Gao, Ge; Lan, Jingbo; Chen, Lijuan
Tetrahedron, 2010 , vol. 66, # 21 p. 3695 - 3701
反应条件
triethylamine in dichloromethane 1.) RT, overnight, 2.) reflux, 30 min;
参考文献
Liebeskind, Lanny S.; Yu, Marvin S.; Yu, Richard H.; Wang, Jianying; Hagen, Karl S.
Journal of the American Chemical Society, 1993 , vol. 115, # 20 p. 9048 - 9055
反应条件
triethylamine in toluene T=-30 - 20°C;
参考文献
Labille, Marie-Christine; Janousek, Zdenek; Viehe, Heinz G.
Tetrahedron, 1991 , vol. 47, # 38 p. 8161 - 8166
