反应条件
1: With AlCl3, aluminium chloride in dichloromethane T=0°C; 1 h; Inert atmosphere; 2: With p-toluenesulfonyl chloride in dichloromethane T=20°C; 48 h; Inert atmosphere; 3: With 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=20°C; 2 h; Inert atmosphere;
参考文献
ELAN PHARMACEUTICALS, INC.; GALEMMO, Robert, A., Jr.; ARTIS, Dean, Richard; YE, Xiaocong, Michael; AUBELE, Danielle, L.; TRUONG, Anh, P.; BOWERS, Simeon; HOM, Roy, K.; ZHU, Yong-Liang; NEITZ, R., Jeffrey; SEALY, Jennifer; ADLER, Marc; BEROZA, Paul; ANDERSON, John, P.
Patent: WO2011/79114 A1, 2011 ;
Location in patent: Page/Page column 107; 108 ;
WO 2011/079114 A1
