N-苄氧羰基-D-亮胺酸合成路线 （共 21 条）
反应条件
sodium hydroxide in water T=20°C; 2 h;
参考文献
Frelek, Jadwiga; Fryszkowska, Anna; Kwit, Marcin; Ostaszewski, Ryszard
Tetrahedron Asymmetry, 2006 , vol. 17, # 17 p. 2469 - 2478
反应条件
citrate buffer; dl-cysteine hydrochloride; papain T=50°C; 24 h;
参考文献
Moriniere, Jean-Luc; Danree, Bernard; Guy, Alain
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 347 - 358
反应条件
phosphate buffer; α-chymotrypsin in dimethyl sulfoxide T=30°C; pH=8.0; 1 h;
参考文献
Salam, Sayed Mohiuddin Abdus; Kagawa, Ken-Ichi; Kawashiro, Katsuhiro
Tetrahedron Asymmetry, 2006 , vol. 17, # 1 p. 22 - 29
反应条件
phosphate buffer; α-chymotrypsin in dimethyl sulfoxide T=-24°C; pH=8.0; 72 h;
参考文献
Salam, Sayed Mohiuddin Abdus; Kagawa, Ken-Ichi; Kawashiro, Katsuhiro
Tetrahedron Asymmetry, 2006 , vol. 17, # 1 p. 22 - 29
反应条件
antibody 3G2; Tris buffer; water in dimethyl sulfoxide T=25°C; Rate constant;
参考文献
Tanaka, Fujie; Kinoshita, Keiko; Tanimura, Ryuji; Fujii, Ikuo
Journal of the American Chemical Society, 1996 , vol. 118, # 10 p. 2332 - 2339
反应条件
jones' reagent in acetone T=0°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
chromium(VI) oxide; sulfuric acid in water; acetone Yield given;
参考文献
Fitzner, Jeffrey N.; Shea, Regan G.; Fankhauser, John E.; Hopkins, Paul B.
Journal of Organic Chemistry, 1985 , vol. 50, # 3 p. 417 - 419
反应条件
sodium hydrogencarbonate; sodium carbonate in water; acetonitrile T=50°C; Substitution; pH=9.5; 1 h;
参考文献
Mitulovi, Goran; Laemmerhofer, Michael; Maier; Lindner, Wolfgang
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 5 p. 449 - 461
反应条件
1: 59 percent / N-chlorosuccinimide, Et3N / methanol / 0 °C 2: 1.) O3, 2.) (CH3)2S / 1.) CH2Cl2, CH3OH, -78 deg C, 2.) CH2Cl2, CH3OH, from -78 deg C to 25 deg C 3: CrO3, H2SO4 / H2O; acetone View Scheme
参考文献
Fitzner, Jeffrey N.; Shea, Regan G.; Fankhauser, John E.; Hopkins, Paul B.
Journal of Organic Chemistry, 1985 , vol. 50, # 3 p. 417 - 419
反应条件
1: 1.) O3, 2.) (CH3)2S / 1.) CH2Cl2, CH3OH, -78 deg C, 2.) CH2Cl2, CH3OH, from -78 deg C to 25 deg C 2: CrO3, H2SO4 / H2O; acetone View Scheme
参考文献
Fitzner, Jeffrey N.; Shea, Regan G.; Fankhauser, John E.; Hopkins, Paul B.
Journal of Organic Chemistry, 1985 , vol. 50, # 3 p. 417 - 419
