1-萘-1-基丙-1-酮合成路线 （共 32 条）
反应条件
Mn(NO3)2; oxygen; cobalt(II) nitrate hexahydrate in acetic acid T=100°C; 6 h;
参考文献
Minisci, Francesco; Recupero, Francesco; Fontana, Francesca; Bjorsvik, Hans-Rene; Liguori, Lucia
Synlett, 2002 , # 4 p. 610 - 612
参考文献
Rousset
Bulletin de la Societe Chimique de France, 1896 , vol. <3> 15, p. 61
反应条件
1: in tetrahydrofuran
2: With water
Acidic conditions;
参考文献
Fuglseth, Erik; Otterholt, Eli; Hogmoen, Hanne; Sundby, Eirik; Charnock, Colin; Hoff, Bard Helge
Tetrahedron, 2009 , vol. 65, # 47 p. 9807 - 9813
反应条件
AlCl3, aluminium chloride
T=35°C; Friedel-Crafts Acylation; Inert atmosphere;
参考文献
Sero, Luc; Calard, Francois; Sanguinet, Lionel; Levillain, Eric; Richomme, Pascal; Seraphin, Denis; Derbre, Severine
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 21 p. 6716 - 6720
反应条件
carbon monoxide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; selenium in tetrahydrofuran
T=120°C; P=22800 Torr; 24 h;
参考文献
Nishiyama, Yutaka; Inoue, Jun; Teranishi, Kazuyo; Moriwaki, Masami; Hamanaka, Sawako
Tetrahedron Letters, 1992 , vol. 33, # 42 p. 6347 - 6350
反应条件
1: in 1,2-dichloro-ethane
T=35 - 50°C; 3 h;
2: With hydrogenchloride in water; 1,2-dichloro-ethane
参考文献
SHIKOKU CHEMICALS CORPORATION
Patent: WO2005/121101 A1, 2005 ;
Location in patent: Page/Page column 21-22 ;
反应条件
1: 1-Bromonaphthalene With magnesium in tetrahydrofuran
T=20°C; Inert atmosphere;
2: N-methoxy-N-methylpropionamide in tetrahydrofuran
T=-20 - 20°C; Inert atmosphere;
3: With water in tetrahydrofuran
参考文献
Ueno, Satoshi; Shimizu, Ryosuke; Kuwano, Ryoichi
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 4543 - 4545
Angewandte Chemie, 2009 , vol. 121, p. 4613 - 4615
反应条件
acridine acid; 2-methylpropane-2-thiol in benzene
2 h; Irradiation;
参考文献
Okada, Keiji; Okubo, Katsura; Oda, Masaji
Tetrahedron Letters, 1989 , vol. 30, # 48 p. 6733 - 6736
反应条件
1: in diethyl ether
17 h; Heating / reflux;
2: With hydrogenchloride in diethyl ether; water
1 h; Heating / reflux;
参考文献
PROSIDION LIMITED
Patent: WO2006/85118 A2, 2006 ;
Location in patent: Page/Page column 23 ;
WO 2006/085118 A2
反应条件
[Cp*Ru(CNCH3)3]+PF6-; potassium carbonate in acetonitrile
1 h; Inert atmosphereReflux;
参考文献
Bouziane, Asmae; Carboni, Bertrand; Bruneau, Christian; Carreaux, Francois; Renaud, Jean-Luc
Tetrahedron, 2008 , vol. 64, # 51 p. 11745 - 11750
