4-乙酰氧基-2-氮杂环丁酮合成路线 （共 46 条）
反应条件
2,2,6,6-tetramethyl-piperidine; copper (I) cyanide; diethylaluminium chloride
further αβ-unsaturated ketones, various reagents; Product distribution;
参考文献
Greengrass; Nobbs
Tetrahedron Letters, 1981 , vol. 22, # 52 p. 5339 - 5340
反应条件
in water; acetone
T=0°C; 0.5 h;
参考文献
Branch, Clive L.; Pearson, Michael J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1097 - 1100
反应条件
sodium ethanolate in water
T=0°C; 2 h;
参考文献
Shibuya, Masayuki; Kubota, Seiju
Heterocycles, 1981 , vol. 15, # 1 p. 489 - 492
反应条件
aluminium; aluminum tri-bromide; lead(II) bromide in tetrahydrofuran
1.5 h; Ambient temperature;
参考文献
Tanaka,Hideo; Yamashita, Shiro; Ikemoto, Youichi; Torii, Sigeru
Tetrahedron Letters, 1988 , vol. 29, # 14 p. 1721 - 1724
反应条件
boron trifluoride in diethyl ether; dichloromethane
参考文献
Crombie, Leslie; Haigh, David; Jones, Raymond C. F.; Mat-Zin, Ab. Rasid
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 17 p. 2055 - 2068
反应条件
copper(l) iodide
1.) THF, -15 deg C, 20 min. 2.) - 30 to 25 deg C, 1 h; Multistep reaction;
参考文献
Hua, Duy H.; Verma, Akhilkumar
Tetrahedron Letters, 1985 , vol. 26, # 5 p. 547 - 550
反应条件
trimethylsilyl trifluoromethanesulfonate; triethylamine
1) CH2Cl2, 15 h; 2) CH2Cl2, 0 deg C, 2 h; 3) MeOH, 0 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Barrett, Anthony G. M.; Baugh, Simon P. D.; Christopher Braddock; Flack, Kevin; Gibson, Vernon C.; Giles, Matthew R.; Marshall, Edward L.; Procopiou, Panayiotis A.; White, Andrew J. P.; Williams, David J.
Journal of Organic Chemistry, 1998 , vol. 63, # 22 p. 7893 - 7907
反应条件
triethylamine in diethyl ether
T=0°C; 2 h;
参考文献
Attrill; Barrett; Quayle; et al.
Journal of Organic Chemistry, 1984 , vol. 49, # 10 p. 1679 - 1682
参考文献
Alcaide, Benito; Polanco, Concepcion; Sierra, Miguel A.
Tetrahedron Letters, 1996 , vol. 37, # 38 p. 6901 - 6904
反应条件
boron trifluoride diethyl etherate in dichloromethane
3 h;
参考文献
Imuta; Uyeo; Yoshida
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 3 p. 658 - 662
