3,3-二甲基-1-氯丁烷合成路线 （共 54 条）
反应条件
in neat (no solvent) (C2H5)3SiH and (CH3)3CCH2CH2Cl in presence of AlCl3 at room temp.;;
参考文献
Whitmore, F. C.; Pietrusza, E. W.; Sommer, L. H.
Journal of the American Chemical Society, 1947 , vol. 69, p. 2108 - 2110
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Gmelin Handbook: Si: MVol.C, 34, page 106 - 108
参考文献
Whitmore; Pietrusza; Sommer
Journal of the American Chemical Society, 1947 , vol. 69, p. 2109
参考文献
Universal Oil Prod.Co.
Patent: US2404927 , 1943 ;
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Schmerling
Journal of the American Chemical Society, 1944 , vol. 66, p. 1423
反应条件
T=25°C; weitere Produkte: 2.2-Dimethyl-butan, Pentan;
参考文献
Schmerling
Journal of the American Chemical Society, 1945 , vol. 67, p. 1778
反应条件
1: 58 percent / Mg / diethyl ether / 1.5 h / Heating 2: 64 percent / sulfuric acid / 18 h / Heating View Scheme
参考文献
Braendstroem
Acta Chemica Scandinavica (1947-1973), 1959 , vol. 13, p. 608
反应条件
1: potassium hydroxide; polyethylene glycol / 120 - 190 °C 2: aqueous hydrogen peroxide; formic acid / und Erwaermen des Reaktionsprodukts mit wss.Natronlauge View Scheme
参考文献
Braendstroem
Acta Chemica Scandinavica (1947-1973), 1959 , vol. 13, p. 608
反应条件
1: (i) Mg, (ii) /BRN= 102378/ 2: PBr3 3: (i) Mg, (ii) /BRN= 1900390/ View Scheme
参考文献
Dolgii,I.E.; Meshcheryakov,A.P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1966 , p. 1935 - 1939
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , # 11 p. 2004 - 2009
参考文献
Desai,V.R. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1970 , p. 386 - 388
反应条件
1: 68 percent / KI / dimethylsulfoxide / 12 h / 95 °C 2: 63 percent / aq. KOH / ethanol / 12 h / Heating 3: 76 percent / LiAlH4 / diethyl ether / 12 h / Heating View Scheme
参考文献
Sasse, Astrid; Ligneau, Xavier; Rouleau, Agnes; Elz, Sigurd; Ganellin, C. Robin; Arrang, Jean-Michel; Schwartz, Jean-Charles; Schunack, Walter; Stark, Holger
Journal of Medicinal Chemistry, 2002 , vol. 45, # 18 p. 4000 - 4010
反应条件
magnesium in diethyl ether Grignard reaction; 1.5 h; Heating;
参考文献
Tilley, Leon J.; Shiner Jr.
Journal of Physical Organic Chemistry, 1999 , vol. 12, # 7 p. 564 - 576
