2,8,9-三氧杂-5-氮杂-1-硅杂双环[3.3.3]十一烷合成路线 (共 17 条)
反应条件
in chloroform 1.5 h; Heating;
参考文献
Voronkov; Kuznetsova; Baryshok
Russian Journal of General Chemistry, 2002 , vol. 72, # 7 p. 1148 - 1149
反应条件
in tetrahydrofuran; hexane T=0°C; 24 h; other organometallic compounds, var. temperature, time, 12-crown-4 as reagent; Product distribution;
参考文献
Cerveau, G.; Chuit, C.; Corriu, R. J. P.; Nayyar, N. K.; Reye, C.
Journal of Organometallic Chemistry, 1990 , vol. 389, # 2 p. 159 - 168
反应条件
in tetrahydrofuran T=20°C; 20 h;
参考文献
Journal of Organometallic Chemistry, , vol. 389, # 2 p. 159 - 168
反应条件
in tetrahydrofuran T=20°C; 20 h;
参考文献
Journal of Organometallic Chemistry, , vol. 389, # 2 p. 159 - 168
反应条件
1,4-diaza-bicyclo[2.2.2]octane; [Rhacetylacetonate(1,5-cyclooctadiene)] in N,N-dimethyl-formamide T=80°C; 16 h; Product distribution; Further Variations:CatalystsReagentsReaction partners;
参考文献
Synthesis, , # 19 p. 2944 - 2946
反应条件
chloroform; dibenzoyl peroxide T=60°C; 10 h;
参考文献
Voronkov, M. G.; Baryshok, V. P.; Petukhov, L. P.; Rakhlin, V. I.; Mirskov, R. G.; Pestunovich, V. A.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 39 - 56
反应条件
1: heptafluoroiodopropane / acetonitrile / 0.5 h / 20 °C / Irradiation 2: CH2Cl2 / 3 h / 20 °C / Irradiation View Scheme
参考文献
Voronkov, M. G.; Baryshok, V. P.; Petukhov, L. P.; Rakhlin, V. I.; Mirskov, R. G.; Pestunovich, V. A.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 39 - 56
反应条件
phenolated sodium in xylene
参考文献
Voronkov,M.G.; Zelchan,G.I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1969 , vol. 5, # 1 p. 34 - 38
Khimiya Geterotsiklicheskikh Soedinenii, 1969 , vol. 5, # 1 p. 43 - 48
反应条件
triphenyl methyl bromide in various solvent(s) T=20°C; 2.5 h;
参考文献
Voronkov, M. G.; Baryshok, V. P.; Petukhov, L. P.; Rakhlin, V. I.; Mirskov, R. G.; Pestunovich, V. A.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 39 - 56
反应条件
C3F7I in acetonitrile T=20°C; 0.5 h; Irradiation; Yield given;
参考文献
Voronkov, M. G.; Baryshok, V. P.; Petukhov, L. P.; Rakhlin, V. I.; Mirskov, R. G.; Pestunovich, V. A.
Journal of Organometallic Chemistry, 1988 , vol. 358, p. 39 - 56