1,2-双(二氯磷基)-乙烷合成路线 （共 18 条）
参考文献
Chatt, Joseph; Hussain, Wasif; Leigh, G. Jeffery; Ali, Hapipah Mohd.; Pickett, Christopher J.; Rankin, Douglas A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1985 , p. 1131 - 1136
反应条件
magnesium
1.) THF, 30 deg C, 2 h, 2.) THF, from -80 deg C to RT, overnight; Yield given. Multistep reaction;
参考文献
Fischer, Reinald; Langer, Jens; Malassa, Astrid; Walther, Dirk; Goerls, Helmar; Vaughan, Gavin
Chemical Communications, 2006 , # 23 p. 2510 - 2512
反应条件
1: 2-methoxybromobenzene With n-butyllithium in tetrahydrofuran; hexane
T=-50°C; 0.75 h;
2: DPPECl4 in tetrahydrofuran; diethyl ether; hexane
T=-50 - 20°C; Further stages.;
参考文献
Shultz; DeSimone; Brookhart
Journal of the American Chemical Society, 2001 , vol. 123, # 37 p. 9172 - 9173
反应条件
in tetrahydrofuran
1.5 h; Heating;
参考文献
Cloke, F. Geoffrey N.; Gibson, Vernon C.; Green, Malcolm L. H.; Mtetwa, Victor S. B.; Prout, Keith
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 2227 - 2230
反应条件
in pentane
1.) -78 deg C, 8 h, 2.) room temp., overnight;
参考文献
Benn, R.; Jolly, P. W.; Joswig, T.; Mynott, R.; Schick, K.-P.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1986 , vol. 41, # 6 p. 680 - 691
反应条件
in diethyl ether
T=-30 - 20°C; 2 h; Yield given;
参考文献
Podlahova, Jana; Podlaha, Jaroslav
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 7 p. 2049 - 2053
反应条件
n-butyllithium in diethyl ether
参考文献
Laitinen, Riitta H.; Losonczi, Judit; Pursiainen, Jouni; Ahlgren, Markku
Acta Chemica Scandinavica, 1997 , vol. 51, # 6-7 p. 804 - 806
反应条件
n-butyllithium in diethyl ether; hexane
T=20°C; 1 h;
参考文献
Chatt, Joseph; Hussain, Wasif; Leigh, G. Jeffery; Ali, Hapipah Mohd.; Pickett, Christopher J.; Rankin, Douglas A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1985 , p. 1131 - 1136
