1,6,6-三(苯基)己基苯合成路线 （共 16 条）
反应条件
magnesium in tetrahydrofuran; water
参考文献
Xerox Corporation
Patent: US5487848 A1, 1996 ;
反应条件
ethanol; nickel; benzene
Hydrogenation;
参考文献
Cadiot; Willemart
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 229, p. 130
Bulletin de la Societe Chimique de France, 1951 , p. 100,103
反应条件
hydrogen; nickel in tetrahydrofuran
参考文献
Kuhn,R.; Fischer,H.
Chemische Berichte, 1961 , vol. 94, p. 3060 - 3071
反应条件
hydrogenchloride; acetic acid; zinc
参考文献
Vorlaender; Rack; Leister
Chemische Berichte, 1923 , vol. 56, p. 1134
反应条件
1: 89 percent / silver perchlorate / 1,2-dichloro-ethane / 14 h / Ambient temperature
2: 15.7 percent / sodium hydride / tetrahydrofuran / 17 h / Ambient temperature
3: 7.7 percent / Raney Ni (W-2) / ethanol / 6 h / Heating
View Scheme
参考文献
Hori, Mikio; Kataoka, Tadashi; Shimizu, Hiroshi; Aoki, Harumi
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 10 p. 3816 - 3825
反应条件
diethyl ether; ammonia; 4-chloro-butyl chloride
参考文献
Hauser et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 397
反应条件
hydrogenchloride; acetic acid; zinc
参考文献
Vorlaender; Rack; Leister
Chemische Berichte, 1923 , vol. 56, p. 1134
反应条件
1,4-dioxane; potassium-sodium
anschliessende Behandlung mit Aethanol;
参考文献
Wittig; Leo
Chemische Berichte, 1930 , vol. 63, p. 943,947
反应条件
1: KOH; acetic acid anhydride; diethyl ether / 0 °C
2: Raney nickel; ethanol; benzene / Hydrogenation
View Scheme
参考文献
Cadiot; Willemart
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1949 , vol. 229, p. 130
Bulletin de la Societe Chimique de France, 1951 , p. 100,103
反应条件
(i) NaNH2, HMPT, THF, (ii) /BRN= 1071199/; Multistep reaction;
参考文献
Cuvigny,T.; Normant,H.
Bulletin de la Societe Chimique de France, 1965 , p. 1872 - 1881
