反应条件
in diethyl ether org. compd. soln. addn. to Ge-compd. soln., mixt. stirring (12 h, room temp.), hydrolysis (HCl 5percent); org. phase drying over Na2SO4, concn. (reduced pressure), residue treatment with ether/pentane, crystn. at -30°C (2 d), crystals isolation (filtration); elem. anal.;
参考文献
Riviere, P.; Castel, A.; Abdennadher, C.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 82, # 1-4 p. 181 - 194
