3,4,5,6-四溴邻二甲苯合成路线 （共 9 条）
反应条件
bromine; iron in dichloromethane T=0 - 20°C; 2 h;
参考文献
Miller, Glen P.; Kaur, Irvinder
Patent: US2011/130593 A1, 2011 ;
Location in patent: Page/Page column 6 ;
反应条件
aluminium durch Bromieren;
参考文献
Klages; Sommer
Chemische Berichte, 1906 , vol. 39, p. 2312
参考文献
Pajeau
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1936 , vol. 202, p. 1795
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1937 , vol. 204, p. 1203
反应条件
bromine; iron 3.5 h; Ambient temperature; Product distribution;
参考文献
Kovalev, V. V.; Knyazeva, I. V.; Shokova, E. A.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 692 - 696
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 4 p. 776 - 780
参考文献
I.G. Farbenind.
Patent: DE595461 , 1929 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 20, p. 1375
参考文献
Jacobsen
Chemische Berichte, 1884 , vol. 17, p. 2374
参考文献
Bluemlein
Chemische Berichte, 1884 , vol. 17, p. 2494
反应条件
1: 88 percent / N-bromosuccinimide, azobis(isobutyronitrile) / CCl4 / 24 h / Heating; Irradiation
2: 63 percent / NaOH / CCl4; ethanol; H2O / 2 h / Heating
3: 72 percent / tBuOK / dimethylsulfoxide / 1 h / Ambient temperature
View Scheme
参考文献
Kreher, Richard P.; Herd, Karl Josef
Chemische Berichte, 1988 , vol. 121, p. 1827 - 1832
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
24 h; Heating;
参考文献
Kreher, Richard P.; Kalischko, Juergen
Chemische Berichte, 1991 , vol. 124, # 3 p. 645 - 654
