(2-硝基-苯基)-丙炔酸乙酯合成路线 （共 5 条）
反应条件
sodium hydride in ethylene glycol dimethyl ether T=0 - 20°C; Horner-Wadsworth-Emmons olefination; 1.5 h;
参考文献
Yamamoto, Yoshihiko; Yamada, Satoshi; Nishiyama, Hisao
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 701 - 706
反应条件
nitric acid T=-30°C;
参考文献
Baker; Cooper; Ingold
Journal of the Chemical Society, 1928 , p. 431
参考文献
Rice, Craig R.; Wallis, John D.
Journal of the Chemical Society, Chemical Communications, 1993 , # 6 p. 572 - 574
反应条件
1: anhydrous copper acetate / methanol / 3 h / 28 °C / Inert atmosphere 2: MoO2Cl2(dmf)2; triphenylphosphine / toluene / 4 h / 80 °C / Inert atmosphere View Scheme
参考文献
Yamamoto, Yoshihiko; Yamada, Satoshi; Nishiyama, Hisao
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 701 - 706
反应条件
1: anhydrous copper acetate / methanol / 3 h / 28 °C / Inert atmosphere 2: MoO2Cl2(dmf)2; triphenylphosphine / toluene / 4 h / 80 °C / Inert atmosphere View Scheme
参考文献
Yamamoto, Yoshihiko; Yamada, Satoshi; Nishiyama, Hisao
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 701 - 706
