1-二甲基呋喃-1-3-酮合成路线 (共 26 条)
反应条件
dimethyl amine in acetone
参考文献
Bayer Aktiengesellschaft
Patent: US5401869 A1, 1995 ;
参考文献
AUSPEX PHARMACEUTICALS, INC.
Patent: US2010/317655 A1, 2010 ;
Location in patent: Page/Page column 14 ;
参考文献
Kozmin, Sergey A.; Janey, Jacob M.; Rawal, Viresh H.
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3039 - 3052
反应条件
in dichloromethane T=20°C; Substitution; 12 h;
参考文献
Paczkowski, Ralph; Maichle-Moessmer, Caecilia; Maier, Martin E.
Organic Letters, 2000 , vol. 2, # 25 p. 3967 - 3969
反应条件
triethylamine; triphenylphosphine in dichloromethane
参考文献
Kozmin, Sergey A.; Rawal, Viresh H.
Journal of Organic Chemistry, 1997 , vol. 62, # 16 p. 5252 - 5253
反应条件
dichloro bis(acetonitrile) palladium(II); triethylamine in acetonitrile 0.5 h; Heating;
参考文献
Murahashi, Shun-Ichi; Mitsue, Yo; Tsumiyama, Tatsuo
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3285 - 3290
参考文献
Markova, N. K.; Zaichenko, Yu. A.; Tsil'ko, A. E.; Maretina, I. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 876 - 880
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 5 p. 962 - 968
反应条件
in isopropyl alcohol 1 h; Heating;
参考文献
Krasnaya, Zh. A.; Bogdanov, V. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 10 p. 2057 - 2065
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 10 p. 2348 - 2356
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 15 min, 2.) THF, hexane, -45 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 52, # 13 p. 2929 - 2930
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 991,994; engl. Ausg. S. 883, 885