S-三苯甲基-L-半胱氨酸合成路线 （共 22 条）
反应条件
1: With trifluoroacetic acid 2 h; 2: With sodium acetate; sodium hydroxide in diethyl ether; water T=0°C; pH=5 - 6;
参考文献
Silvia, Vertuani; Baldisserotto, Anna; Scalambra, Emanuela; Malisardi, Gemma; Durini, Elisa; Manfredini, Stefano
European Journal of Medicinal Chemistry, 2012 , vol. 50, p. 383 - 392
反应条件
in N,N-dimethyl-formamide T=20°C; 48 h;
参考文献
Marquette University; University of Wisconsin - Milwaukee
Patent: US7829709 B1, 2010 ;
Location in patent: Page/Page column 19-20 ;
反应条件
boron trifluoride diethyl etherate; acetic acid T=20°C; 5 h;
参考文献
Jin, Hui-Juan; Lu, Jing; Wu, Xue
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 11 p. 3465 - 3469
反应条件
sodium azide in N,N-dimethyl-formamide T=50°C; 9 h;
参考文献
Chen, Chun-Chi; Rajagopal, Basker; Liu, Xuan Yu; Chen, Kuan Lin; Tyan, Yu-Chang; Lin, Fui; Lin, Po-Chiao
Amino Acids, 2014 , vol. 46, # 2 p. 367 - 374
反应条件
in N,N-dimethyl-formamide T=20°C; 48 h;
参考文献
Zheng, Yan; Duanmu, Chuansong; Gao, Yong
Organic Letters, 2006 , vol. 8, # 15 p. 3215 - 3217
反应条件
magnesium bromide in acetonitrile T=40 - 50°C; Product distribution / selectivity;
参考文献
WO2007/9944 A1, ;
Page/Page column 31-32 ;
参考文献
WO2006/102243 A2, ;
Page/Page column 63 ;
WO 2006/102243 A2
反应条件
diethyl ether; diethylamine
参考文献
Bulletin de la Societe Chimique de France, , p. 698
反应条件
triethylsilane in dichloromethane; trifluoroacetic acid 1 h; Ambient temperature;
参考文献
Pearson, Daniel A.; Blanchette, Mary; Baker, Mary Lou; Guindon, Cathy A.
Tetrahedron Letters, 1989 , vol. 30, # 21 p. 2739 - 2742
反应条件
dimercaptoethane; methoxybenzene; Tl(OCOCF3)3 1.) trifluoroacetic acid, 0 deg c, 60 min; 2.) 40 deg C, 5 h, pH=7.5 adjusted with 5percent NH4OH;
参考文献
Fujii; Otaka; Funakoshi; Bessho; Watanabe; Akaji; Yajima
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 6 p. 2339 - 2347
