1,4-二硫杂螺[4.5]癸烷-6-酮合成路线 （共 6 条）
反应条件
water; 1-Fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate in tetrahydrofuran; dichloromethane T=23°C;
参考文献
Kiselyov; Strekowski; Semenov
Tetrahedron, 1993 , vol. 49, # 11 p. 2151 - 2158
反应条件
toluene-4-sulfonic acid in benzene Heating;
参考文献
Takemura, Tetsuo; Hosoya, Yoshiko; Mori, Nobuo
Canadian Journal of Chemistry, 1990 , vol. 68, # 4 p. 523 - 529
反应条件
triarylamin-radicalcation in water; acetonitrile electrochemical oxydation;
参考文献
Fjeldskaar, Inger Reidun; Skatteboel, Lars
Acta Chemica Scandinavica, 1991 , vol. 45, # 4 p. 410 - 417
反应条件
1: sulphuryl chloride / CCl4 / 1 h / 0 °C 2: 1.) triethylamine, 2.) silica gel (Merk Kieselgel H, type 60), water / 1.) CCl4, 0 deg C -> room temperature View Scheme
参考文献
Bulman-Page, Philip C.; Ley, Steven V.; Morton, Judith A.; Williams, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 457 - 461
反应条件
toluene-4-sulfonic acid; benzene Entfernen des entstehenden Wassers;
参考文献
Jaeger; Smith
Journal of the Chemical Society, 1955 , p. 160,164
反应条件
1: 96 percent / sodium borohydride / ethanol / 1 h / 20 °C 2: 7 percent / HN3 / DEAD; TPP / benzene / 48 h / 20 °C View Scheme
参考文献
Afonso, Carlos A. M.; Barros, M. Teresa; Maycock, Christopher D.
Tetrahedron, 1999 , vol. 55, # 3 p. 801 - 814
