反应条件
in dichloromethane N2 atmosphere, addn. of soln. of stannyl compound to soln. of borane at -50°C (1 h) with stirring, slow warming to room temp., stirring (room temp., 2 d); removement of solvent (25°C, 12 Torr), pptn. of Me2SnBr2 (petroleum ether, -30°C, 4-6 h), filtration, removement of Me2SnBr2 (25°C, 1E-6 Torr), fractional distillation (50°C, 1E-6 Torr); elem. anal.;
参考文献
Diemer, Stefan; Noeth, Heinrich; Storch, Wolfgang
European Journal of Inorganic Chemistry, 1999 , # 9 p. 1765 - 1780
