1,1,1-三氟-甲烷磺酸二甲基[[(三氟甲基)磺酰基]氧基]硅烷基酯合成路线 (共 11 条)
参考文献
Matyjaszewski, K.; Chen, Y. L.
Journal of Organometallic Chemistry, 1988 , vol. 340, p. 7 - 12
反应条件
in chloroform-d1; dichloromethane 0.0833333 h;
参考文献
Henry, Courtney; Brook, Michael A.
Tetrahedron, 1994 , vol. 50, # 39 p. 11379 - 11390
参考文献
Uhlig, Wolfram; Tzschach, Alfred
Zeitschrift fuer Chemie (Stuttgart, Germany), 1988 , vol. 28, # 3 p. 104 - 106
反应条件
T=0 - 20°C; 0.5 h; Inert atmosphereSchlenk technique;
参考文献
Martin, Sara E. S.; Watson, Donald A.
Journal of the American Chemical Society, 2013 , vol. 135, # 36 p. 13330 - 13333
参考文献
Schmeisser, M.; Sartori, P.; Lippsmeier, B.
Chemische Berichte, 1970 , vol. 103, p. 868 - 879
反应条件
in diethyl ether T=0°C;
参考文献
Uhlig, Wolfram
Helvetica Chimica Acta, 1994 , vol. 77, p. 972 - 980
反应条件
in chloroform-d1 1 h; Ambient temperature; Yield given;
参考文献
Matyjaszewski, K.; Chen, Y. L.
Journal of Organometallic Chemistry, 1988 , vol. 340, p. 7 - 12
反应条件
T=20°C; Inert atmosphere;
参考文献
Suslova, Elena N.; Albanov, Alexandr I.; Shainyan, Bagrat A.
Journal of Organometallic Chemistry, 2009 , vol. 694, # 3 p. 420 - 426
反应条件
in diethyl ether Ar-atmosphere; mixing at -70°C, stirring and warming to 0°C (3 h); evapn. (vac., 0°C), toluene addn., filtration off of Li-triflate (cooling), evapn. (vac.); elem. anal.;
参考文献
Uhlig, W.
Journal of Organometallic Chemistry, 1991 , vol. 409, # 3 p. 377 - 383
反应条件
in diethyl ether Ar-atmosphere; mixing at -70°C, stirring and warming to 0°C (3 h); evapn. (vac., 0°C), toluene addn., filtration off of Li-triflate (cooling), evapn. (vac.); elem. anal.;
参考文献
Uhlig, W.
Journal of Organometallic Chemistry, 1991 , vol. 409, # 3 p. 377 - 383