反应条件
boron trifluoride diethyl etherate in dichloromethane under N2, a flask is charged with n-Bu3SnCH2OH, (MeO)2CH2, powdered 4-Å molecular sieves and CH2Cl2, boron trifluoride etherate is then added in one portion, suspn. is kept standing for 18 h; filtered, filtrate extd. with satd. NaHCO3 soln. and satd. NaCl soln., dried over Na2SO4, filtered, concd., distn.; elem. anal.;
参考文献
Danheiser,R.L.; Gee,S.K.; Perez,J.J.
Journal of the American Chemical Society, 1986 , vol. 108, p. 806
