4-硝基-苯甲酰基叠氮化物合成路线 (共 51 条)
反应条件
sodium azide; C39H32Cl2OP2Pd*CH2Cl2; potassium carbonate in tetrahydrofuran; hexane; water
T=20°C; Heck Reaction; P=760.051 Torr; Reagent/catalyst;
参考文献
Miloserdov, Fedor M.; McMullin, Claire L.; Belmonte, Marta Martinez; Benet-Buchholz, Jordi; Bakhmutov, Vladimir I.; Macgregor, Stuart A.; Grushin, Vladimir V.
Organometallics, 2014 , vol. 33, # 3 p. 736 - 752
反应条件
sodium azide; Pd2(dba)5; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran; hexane; water
T=23°C; P=760.051 Torr; 1 h;
参考文献
Miloserdov, Fedor M.; Grushin, Vladimir V.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3668 - 3672
反应条件
sodium azide; FeCl3·6H2O in water; acetone
T=20°C; 0.166667 h;
参考文献
Zhong, Zhiyun; Hu, Jieling; Wang, Xiaoxia; Liu, Junhua; Zhang, Longfeng
Synthetic Communications, 2011 , vol. 41, # 16 p. 2461 - 2467
反应条件
sodium azide in water; acetone
Ambient temperature;
参考文献
Weber, Gunther; Hauptmann, Siegfried; Wilde, Horst; Mann, Gerhard
Synthesis, 1983 , # 3 p. 191 - 192
反应条件
sodium azide; tetrabutylammomium bromide; phenylphosphoric acid dichloride in dichloromethane
2 h; Ambient temperature;
参考文献
Lago, J. M.; Arrieta, A.; Palomo, C.
Synthetic Communications, 1983 , vol. 13, # 4 p. 289 - 296
反应条件
sodium azide; [bis(acetoxy)iodo]benzene in acetonitrile
T=0 - 80°C; 36 h; Inert atmosphere;
参考文献
Li, Xiao-Qiang; Wang, Wei-Kun; Han, Yi-Xin; Zhang, Chi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2588 - 2598
参考文献
Curtius; Struve; Radenhausen
Journal fuer Praktische Chemie (Leipzig), 1895 , vol. <2> 52, p. 232
反应条件
1: toluene / 0.5 h / Heating
2: toluene-4-sulfonic acid / toluene / 0.5 h
View Scheme
参考文献
Curtis, Neville J.
Australian Journal of Chemistry, 1988 , vol. 41, # 4 p. 585 - 595
参考文献
Sah
Recueil des Travaux Chimiques des Pays-Bas, 1940 , vol. 59, p. 231,235
Journal of the Chinese Chemical Society (Peking), 1946 , vol. 13, p. 28,35,40,42,45,47
参考文献
Grammaticakis,P.
Bulletin de la Societe Chimique de France, 1967 , p. 84 - 94