4-硝基-苯甲酰基叠氮化物合成路线 （共 51 条）
反应条件
[Cu(tris(3,5-dimethyl-4-bromopyrazolyl)methane)(MeCN)]BF4 in chloroform T=40°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 133, # 2 p. 191 - 193
反应条件
1: benzene / auf Siedetemperatur 2: acetic acid; benzene View Scheme
参考文献
Naegeli; Tyabji
Helvetica Chimica Acta, 1933 , vol. 16, p. 349,362
Helvetica Chimica Acta, 1934 , vol. 17, p. 931,950
参考文献
Naegeli; Tyabji
Helvetica Chimica Acta, 1933 , vol. 16, p. 349,362
Helvetica Chimica Acta, 1934 , vol. 17, p. 931,950
反应条件
1) toluene, reflux, 0.5 h; 2) toluene, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Corrie, John E. T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 20 p. 2975 - 2982
反应条件
[(tris(3,5-dimethylpyrazolylmethyl)amine)Cu]PF6 T=40°C; 24 h; Inert atmosphereSchlenk technique;
参考文献
Haldon, Estela; Besora, Maria; Cano, Israel; Cambeiro, Xacobe C.; Pericas, Miquel A.; Maseras, Feliu; Nicasio, M. Carmen; Perez, Pedro J.
Chemistry - A European Journal, 2014 , vol. 20, # 12 p. 3463 - 3474
参考文献
Naegeli; Tyabji
Helvetica Chimica Acta, 1933 , vol. 16, p. 349,362
Helvetica Chimica Acta, 1934 , vol. 17, p. 931,950
反应条件
sodium azide in water; acetone
T=22 - 25°C;
参考文献
Brown; Moudachirou
Tetrahedron, 1994 , vol. 50, # 34 p. 10309 - 10320
反应条件
dinitrogen tetraoxide in tetrachloromethane; acetonitrile
T=-30°C; 0.166667 h;
参考文献
Kim, Yong Hae; Kim, Kweon; Shim, Sung Bo
Tetrahedron Letters, 1986 , vol. 27, # 39 p. 4749 - 4752
反应条件
sodium azide; N-halosuccinimide; triphenylphosphine in acetone
T=-30 - 20°C; 0.5 h;
参考文献
Froeyen, Paul
Phosphorus, Sulfur and Silicon and the Related Elements, 1994 , vol. 89, # 1-4 p. 57 - 62
反应条件
manganese(IV) oxide; sodium azide; tetrachlorosilane in dichloromethane
T=0°C;
参考文献
Elmorsy, Saad S.
Tetrahedron Letters, 1995 , vol. 36, # 8 p. 1341 - 1342
