反应条件
1.1: dichloromethane-d2 / 0.17 h / -78 °C / |Inert atmosphere; |Glovebox; |Schlenk technique 1.2: 8 h / -78 - -20 °C / |Inert atmosphere 2.1: dichloromethane-d2 / -78 - -20 °C / |Inert atmosphere; |Glovebox; |Schlenk technique 3.1: dichloromethane-d2 / -78 - -62 °C / |Inert atmosphere; |Glovebox; |Schlenk technique View Scheme
参考文献
Brooner, Rachel E. M.; Brown, Timothy J.; Widenhoefer, Ross A.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 24 p. 6259 - 6261
Angew. Chem., 2013 , vol. 125, # 24 p. 6379 - 6381,3