1-(烯丙基)吡咯烷-2-酮合成路线 (共 19 条)
反应条件
ammonium formate; palladium on activated charcoal in methanol 1.5 h; Heating;
参考文献
Paryzek, Zdzislaw; Koenig, Hanna; Tabaczka, Bartlomiej
Synthesis, 2003 , # 13 p. 2023 - 2026
反应条件
1: With bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride 2: With ruthenium trichloride; sodium periodate 3: in water
参考文献
Alcaide, Benito; Almendros, Pedro; Alonso, Jose M.
Tetrahedron Letters, 2003 , vol. 44, # 48 p. 8693 - 8695
反应条件
Rhodium trichloride 8 h; Heating;
参考文献
Zacuto, Michael J.; Xu, Feng
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6298 - 6300
反应条件
Rhodium trichloride 8 h; Heating;
参考文献
Zacuto, Michael J.; Xu, Feng
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6298 - 6300
反应条件
1: pyrrolidin-2-one With sodium hydride in tetrahydrofuran
2: allyl bromide in tetrahydrofuran
参考文献
Ohmura, Naoya; Nakamura, Asami; Hamasaki, Akiyuki; Tokunaga, Makoto
European Journal of Organic Chemistry, 2008 , # 30 p. 5042 - 5045
反应条件
sodium tetrahydroborate; RhH(CO)(triphenylphosphine)3 in dichloromethane; isopropyl alcohol
T=100°C; P=26220 Torr; 24 h;
参考文献
Zhou, Jian-Qiang; Alper, Howard
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3328 - 3331
反应条件
bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
T=60°C; 1 h;
参考文献
Inoue, Yoshio; Taguchi, Masaaki; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 9 p. 2721 - 2722
反应条件
silver hexafluoroantimonate; ClAu(di(tert-butyl)(1,1′-biphenyl-2-yl)-phosphine) in 1,4-dioxane
T=80°C; 48 h; Inert atmosphere;
参考文献
Mukherjee, Paramita; Widenhoeferst, Ross A.
Organic Letters, 2010 , vol. 12, # 6 p. 1184 - 1187
反应条件
sodium methylate in water; toluene
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: US5081260 A1, 1992 ;
反应条件
1: pyrrolidin-2-one With sodium hydride in tetrahydrofuran; paraffin oil
T=0°C; 0.5 h; Inert atmosphere;
2: 3-iodoprop-1-ene in tetrahydrofuran; paraffin oil
T=0 - 20°C; Inert atmosphere;
参考文献
Curti, Claudio; Ranieri, Beatrice; Battistini, Lucia; Rassu, Gloria; Zambrano, Vincenzo; Pelosi, Giorgio; Casiraghi, Giovanni; Zanardi, Franca
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 11-12 p. 2011 - 2022