3,3',4,4'-四氨基二苯基醚合成路线 （共 14 条）
反应条件
10 Pd/C; hydrogen in methanol T=20°C;
参考文献
Wang, Xiu-Jun; Yang, Ming-Li; Zhang, Lan-Ping; Yao, Tong; Chen, Cheng; Mao, Lian-Gang; Wang, Yin; Wu, Jie
Chinese Chemical Letters, 2014 , vol. 25, # 4 p. 589 - 592
反应条件
1: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 2: 96 percent / aq. NaOH / propan-2-ol / 80 °C 3: 60 percent / NH2NH2; FeCl3; activated charcoal / butan-1-ol / 17 h / 96 - 106 °C View Scheme
参考文献
Wang, Xiu-Jun; Chu, Na-Ying; Wang, Qin-He; Liu, Chao; Jiang, Chun-Guo; Wang, Xiao-Yu; Ikejima, Takashi; Cheng, Mao-Sheng
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 19 p. 6297 - 6300
反应条件
1: 96 percent / aq. NaOH / propan-2-ol / 80 °C 2: 60 percent / NH2NH2; FeCl3; activated charcoal / butan-1-ol / 17 h / 96 - 106 °C View Scheme
参考文献
Wang, Xiu-Jun; Chu, Na-Ying; Wang, Qin-He; Liu, Chao; Jiang, Chun-Guo; Wang, Xiao-Yu; Ikejima, Takashi; Cheng, Mao-Sheng
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 19 p. 6297 - 6300
反应条件
1: 93 percent / chlorobenzene / 2 h / 90 - 95 °C 2: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 3: 96 percent / aq. NaOH / propan-2-ol / 80 °C 4: 60 percent / NH2NH2; FeCl3; activated charcoal / butan-1-ol / 17 h / 96 - 106 °C View Scheme
参考文献
Wang, Xiu-Jun; Chu, Na-Ying; Wang, Qin-He; Liu, Chao; Jiang, Chun-Guo; Wang, Xiao-Yu; Ikejima, Takashi; Cheng, Mao-Sheng
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 19 p. 6297 - 6300
反应条件
1: 92 percent / K2CO3 / dimethylformamide / 10 h / 145 - 150 °C 2: 95 percent / NH2NH2; FeCl3; activated charcoal / dioxane 3: 93 percent / chlorobenzene / 2 h / 90 - 95 °C 4: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 5: 96 percent / aq. NaOH / propan-2-ol / 80 °C 6: 60 percent / NH2NH2; FeCl3; activated charcoal / butan-1-ol / 17 h / 96 - 106 °C View Scheme
参考文献
Pilyugin; Sapozhnikov; Kiseleva; Sapozhnikova; Vorob'eva; Klimakova
Russian Journal of General Chemistry, 2005 , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 95 percent / NH2NH2; FeCl3; activated charcoal / dioxane 2: 93 percent / chlorobenzene / 2 h / 90 - 95 °C 3: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 4: 96 percent / aq. NaOH / propan-2-ol / 80 °C 5: 60 percent / NH2NH2; FeCl3; activated charcoal / butan-1-ol / 17 h / 96 - 106 °C View Scheme
参考文献
Abuzar, Syed; Sharma, Satyavan; Gupta, Suman; Misra, Anuradha; Katiyar, J. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 12 p. 1274 - 1278
反应条件
1: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 2: 96 percent / aq. NaOH / propan-2-ol / 80 °C 3: 60 percent / NH2NH2; FeCl3; activated charcoal / butan-1-ol / 17 h / 96 - 106 °C View Scheme
参考文献
Pilyugin; Sapozhnikov; Kiseleva; Sapozhnikova; Vorob'eva; Klimakova
Russian Journal of General Chemistry, 2005 , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 80 percent / NH2NH2; FeCl3; activated charcoal 2: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 3: 96 percent / aq. NaOH / propan-2-ol / 80 °C 4: 60 percent / NH2NH2; FeCl3; activated charcoal / butan-1-ol / 17 h / 96 - 106 °C View Scheme
参考文献
Pilyugin; Sapozhnikov; Kiseleva; Sapozhnikova; Vorob'eva; Klimakova
Russian Journal of General Chemistry, 2005 , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 93 percent / K2CO3 / dimethylformamide / 10 h / 145 - 150 °C 2: 80 percent / NH2NH2; FeCl3; activated charcoal 3: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 4: 96 percent / aq. NaOH / propan-2-ol / 80 °C 5: 60 percent / NH2NH2; FeCl3; activated charcoal / butan-1-ol / 17 h / 96 - 106 °C View Scheme
参考文献
Pilyugin; Sapozhnikov; Kiseleva; Sapozhnikova; Vorob'eva; Klimakova
Russian Journal of General Chemistry, 2005 , vol. 75, # 10 p. 1509 - 1513
反应条件
1: 80 percent / NH2NH2; FeCl3; activated charcoal 2: 94 percent / HNO3; AcOH; Ac2O / urea / 50 - 60 °C 3: 96 percent / aq. NaOH / propan-2-ol / 80 °C 4: 60 percent / NH2NH2; FeCl3; activated charcoal / butan-1-ol / 17 h / 96 - 106 °C View Scheme
参考文献
Pilyugin; Sapozhnikov; Kiseleva; Sapozhnikova; Vorob'eva; Klimakova
Russian Journal of General Chemistry, 2005 , vol. 75, # 10 p. 1509 - 1513
