2-氯-N,N-二甲基乙酰胺合成路线 （共 38 条）
反应条件
hydrogenchloride in tetrahydrofuran; hexane
参考文献
Love, Christopher; Van Wauwe, Jean Pierre Frans; De Brabander, Marc; Cooymans, Ludwig; Vandermaesen, Nele; Kennis, Ludo Edmond Josephine
Patent: US2003/203897 A1, 2003 ;
反应条件
trichlorophosphate 1.) room temp., 6 h, 2.) 1,2-dichloroethane, room temp., 16 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Synthesis, , # 10 p. 783 - 784
参考文献
Marini-Bettolo; Cavalla
Gazzetta Chimica Italiana, 1954 , vol. 84, p. 896,905
参考文献
Waley; Watson
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, 1949 , vol. 199, p. 499,501
反应条件
trichlorophosphate
T=0 - 20°C; 2.5 h;
参考文献
Gitto, Rosaria; De Luca, Laura; Ferro, Stefania; Russo, Emilio; De Sarro, Giovambattista; Chisari, Mariangela; Ciranna, Lucia; Alvarez-Builla, Julio; Alajarin, Ramon; Buemi, Maria Rosa; Chimirri, Alba
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 3 p. 1040 - 1048
参考文献
Fourneau et al.
Journal de Pharmacie et de Chimie, 1934 , vol. <8> 19, p. 49,50, 52
反应条件
in acetone
T=20°C; 16 h;
参考文献
Reiter, Lawrence A.; Linde, Robert G.
Patent: US2008/76771 A1, 2008 ;
Location in patent: Page/Page column 16 ;
反应条件
sodium hydroxide; tetra(n-hexyl)-ammonium chloride in dichloromethane
T=40 - 42°C; 3 h; Yield given;
参考文献
Occidental Chemical Corporation
Patent: US4922012 A1, 1990 ;
参考文献
Larizza; Brancaccio
Gazzetta Chimica Italiana, 1959 , vol. 89, p. 2402,2404
反应条件
sodium hydride in diethyl ether
Ambient temperature;
参考文献
van der Stelt,C. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1973 , vol. 92, p. 493 - 512
