sodium chloride in diethyl ether; water at 30°C; pouring the reaction mixture into ice-cold satd. aq. NaCl soln.; extrn. with ether; addn. of xylene and removing the ether;
参考文献
Vanderberg, J. T.; Moore, C. E.; Cassaretto, F. P.; Posvic, H.
Analytica Chimica Acta, 1969 , vol. 44, p. 175 - 183
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Gmelin Handbook: B: B-Verb.8, 11.2.3, page 167 - 173
in methanol refluxeed in anhydrous methanol; trimethylamine and methanol are removed under vac. at 70°C;
参考文献
Vanderberg, J. T.; Moore, C. E.; Cassaretto, F. P.; Posvic, H.
Analytica Chimica Acta, 1969 , vol. 44, p. 175 - 183
Full Text View citing articles Show Details
Gmelin Handbook: B: B-Verb.8, 11.2.3, page 167 - 173
