5-甲基呋喃-3-羧酸乙酯合成路线 (共 6 条)
反应条件
1: 56 percent / N-bromosuccinimide, azobis(isobutyronitrile) / CCl4 / 6 h / Heating 2: 1.5 h / Heating View Scheme
参考文献
Pevzner; Ignat'ev; Ionin
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 542 - 547
反应条件
oxygen; acetic acid; bis(acetylacetonato) palladium; cerium(III) chloride in methanol
T=80°C; P=760.051 Torr; 4.5 h;
参考文献
Tamaso, Ken-Ichi; Hatamoto, Yuji; Obora, Yasushi; Sakaguchi, Satoshi; Ishii, Yasutaka
Journal of Organic Chemistry, 2007 , vol. 72, # 23 p. 8820 - 8823
参考文献
Daicel Chemical Industries, Ltd.
Patent: US2007/197806 A1, 2007 ;
Location in patent: Page/Page column 7 ;
参考文献
Daicel Chemical Industries, Ltd.
Patent: US2007/197806 A1, 2007 ;
Location in patent: Page/Page column 8 ;
反应条件
T=190°C; 15 h; Yield given. Yields of byproduct given;
参考文献
Jaworski, Tadeusz; Mizerski, Tadeusz
Polish Journal of Chemistry, 1981 , vol. 55, # 2 p. 317 - 320
参考文献
Jones
Journal of the American Chemical Society, 1955 , vol. 77, p. 4069,4072