3-溴-3-甲基-2-丁酮合成路线 （共 48 条）
反应条件
N-bromosuccinmide; meta-chloroperoxybenzoic acid in tetrachloromethane 5 h; Heating;
参考文献
Sakai, Takashi; Ishikawa, Mutsumi; Amano, Eiichiro; Utaka, Masanori; Takeda, Akira
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 6 p. 2295 - 2297
反应条件
bromine in ethanol T=0 - 10°C;
参考文献
Cardwell; Kilner
Journal of the Chemical Society, 1951 , p. 2430,2440
反应条件
phosphorus tribromide in diethyl ether; water
参考文献
Syntex (U.S.A.) Inc.
Patent: US5447943 A1, 1995 ;
US 5447943 A
反应条件
Sodium bromate; sulfuric acid; sodium bromide in water T=60°C; 0.05 h; Microwave irradiation;
参考文献
Paeaekkoenen, Sanna; Pursiainen, Jouni; Lajunen, Marja
Tetrahedron Letters, 2010 , vol. 51, # 51 p. 6695 - 6699
反应条件
Sodium bromate; sulfuric acid; sodium bromide in water T=33 - 35°C; 0.666667 h; Microwave irradiation;
参考文献
Paeaekkoenen, Sanna; Pursiainen, Jouni; Lajunen, Marja
Tetrahedron Letters, 2010 , vol. 51, # 51 p. 6695 - 6699
参考文献
Blanco,L. et al.
Synthesis, 1976 , p. 194 - 196
反应条件
phosphorus tribromide
参考文献
Arbusow; Winogradowa
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1957 , p. 59
Chem.Abstr., 1956 , p. 9872
参考文献
Orazi; Meseri
Anales de la Asociacion Quimica Argentina (1921-2001), 1950 , vol. 38, p. 300,306
反应条件
bromine 2.) acetone, RT, 3 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Vegh, Daniel; Uher, Michal; Rajniakova, Olga; Dandarova, Miloslava; Kovac, Milan
Collection of Czechoslovak Chemical Communications, 1993 , vol. 58, # 2 p. 404 - 408
反应条件
T=40 - 45°C; unter Belichtung;
参考文献
Catch et al.
Journal of the Chemical Society, 1948 , p. 276
