(三-2-丙烯-1-基硅烷基)-苯合成路线 (共 61 条)
反应条件
1: PTAS With tetrabutyl ammonium fluoride in water; dimethyl sulfoxide T=20°C; 1 h; 2: 4-bromo-aniline With tri-cyclo-hexyl-phosphine; palladium dichloride in water; dimethyl sulfoxide T=80°C; 3 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
反应条件
tetrabutyl ammonium fluoride; palladium dichloride; tri-cyclo-hexyl-phosphine in water; dimethyl sulfoxide T=80°C; 3 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
反应条件
1: PTAS With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: ortho-chlorotoluene With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 16 h;
参考文献
Sahoo, Akhila K.; Nakao, Yoshiaki; Hiyama, Tamejiro
Chemistry Letters, 2004 , vol. 33, # 5 p. 632 - 633
反应条件
tetrabutyl ammonium fluoride; palladium dichloride; tri-cyclo-hexyl-phosphine in water; dimethyl sulfoxide T=80°C; 3 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
反应条件
1: PTAS With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: alpha-chloronaphthalene With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 14 h;
参考文献
Sahoo, Akhila K.; Nakao, Yoshiaki; Hiyama, Tamejiro
Chemistry Letters, 2004 , vol. 33, # 5 p. 632 - 633
反应条件
1: PTAS With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: thien-3-yl chloride With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 12 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1715 - 1727
反应条件
1: PTAS With tetrabutyl ammonium fluoride in water; dimethyl sulfoxide T=20°C; 1 h; 2: 1-bromo-2-chloro-benzene With tri-cyclo-hexyl-phosphine; palladium dichloride in water; dimethyl sulfoxide T=80°C; 10 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1715 - 1727
反应条件
1: PTAS With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: 2-chloro-anisole With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 14 h;
参考文献
Sahoo, Akhila K.; Nakao, Yoshiaki; Hiyama, Tamejiro
Chemistry Letters, 2004 , vol. 33, # 5 p. 632 - 633
反应条件
1: PTAS With tetrabutyl ammonium fluoride in water; dimethyl sulfoxide T=20°C; 1 h; 2: 1-chloro-4-bromobenzene With tri-cyclo-hexyl-phosphine; palladium dichloride in water; dimethyl sulfoxide T=80°C; 12 h;
参考文献
Sahoo, Akhila K.; Nakao, Yoshiaki; Hiyama, Tamejiro
Chemistry Letters, 2004 , vol. 33, # 5 p. 632 - 633
反应条件
1: PTAS With tetrabutyl ammonium fluoride in water; dimethyl sulfoxide T=20°C; 1 h; 2: 1-bromo-3-chlorobenzene With tri-cyclo-hexyl-phosphine; palladium dichloride in water; dimethyl sulfoxide T=80°C; 12 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1715 - 1727