2-氟-4-(4,4,5,5-四甲基-1,3,2-二氧代硼戊烷-2-基)苯基氨基甲酸叔丁酯合成路线 (共 4 条)
反应条件
potassium acetate; PdCl2[dppf] in n-heptane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide
反应条件
in methanol T=20°C; 1 h;
参考文献
WO2007/147574 A1, ;
Page/Page column 56 ;
反应条件
sodium hexamethyldisilazane in tetrahydrofuran; n-heptane; ethyl acetate
参考文献
US2002/156081 A1, ;
US 20020156081 A1
反应条件
1: With hydrogenchloride in 1,4-dioxane; dichloromethane T=30°C; 2.5 h; 2: With sodium hydrogencarbonate in water Product distribution / selectivity;
参考文献
WO2007/147574 A1, ;
Page/Page column 56 ;