4-(二氟甲基)-1-氟苯合成路线 （共 7 条）
反应条件
tetraethyl ammonium fluoride in acetonitrile Ambient temperatureelectrolysis: smooth platinum sheets as the anode and the cathode, Ag/AgClO4 as a reference electrode, 2.5 V, 2.7 F/mol; Further byproducts given;
参考文献
Momota, Kunitaka; Yonezawa, Tetsuo; Mukai, Katsuji; Morita, Masayuki
Journal of Fluorine Chemistry, 1998 , vol. 87, # 2 p. 173 - 178
反应条件
xanthone powder; selectfluor in acetonitrile T=27°C; 24 h; GloveboxIrradiation;
参考文献
Xia, Ji-Bao; Zhu, Chen; Chen, Chuo
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17494 - 17500
反应条件
sulfur(IV) fluoride T=150°C;
参考文献
Kondratenko,N.V. et al.
Zhurnal Organicheskoi Khimii, 1970 , vol. 6, # 7 p. 1423 - 1426,1436 - 1439
反应条件
1: With tripotassium phosphate monohydrate; C28H41ClNPPd in toluene T=100°C; 30 h; Sealed tube; 2: With water; potassium hydroxide in toluene T=100°C; 2 h; Sealed tube;
参考文献
Ge, Shaozhong; Chaladaj, Wojciech; Hartwig, John F.
Journal of the American Chemical Society, 2014 , vol. 136, # 11 p. 4149 - 4152
反应条件
1: With tripotassium phosphate monohydrate; C28H41ClNPPd in toluene T=100°C; 30 h; Sealed tube; 2: With water; potassium hydroxide in toluene T=100°C; 2 h; Sealed tube;
参考文献
Ge, Shaozhong; Chaladaj, Wojciech; Hartwig, John F.
Journal of the American Chemical Society, 2014 , vol. 136, # 11 p. 4149 - 4152
参考文献
Kondratenko,N.V. et al.
Zhurnal Organicheskoi Khimii, 1970 , vol. 6, # 7 p. 1423 - 1426,1436 - 1439
反应条件
silver; tetraethyl ammonium fluoride in acetonitrile Ambient temperaturevarious anode potential and various quantity of electricity; also with Et4NF*3.5HF; Product distribution;
参考文献
Momota, Kunitaka; Yonezawa, Tetsuo; Mukai, Katsuji; Morita, Masayuki
Journal of Fluorine Chemistry, 1998 , vol. 87, # 2 p. 173 - 178
