(二溴甲基)(三甲基)硅烷合成路线 (共 16 条)
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78°C; Yields of byproduct given;
参考文献
Wiberg, Nils; Wagner, Gerhard
Chemische Berichte, 1986 , vol. 119, # 5 p. 1455 - 1466
反应条件
(i) LDA, (ii) /BRN= 1209232/; Multistep reaction;
参考文献
Yoon, Kunsang; Son, David Y.
Journal of Organometallic Chemistry, 1997 , vol. 545-546, p. 185 - 189
反应条件
in tetrahydrofuran T=-80°C;
参考文献
Normant,H.; Villieras,J.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1965 , vol. 260, p. 4535 - 4536
反应条件
(i) iPrMgCl, THF, (ii) /BRN= 1209232/; Multistep reaction;
参考文献
Seyferth,D. et al.
Journal of Organometallic Chemistry, 1970 , vol. 24, p. 647 - 661
反应条件
bei der Photobromierung;
参考文献
Brynolf
Fysiograf.Saellsk.Lund Foerh., 1959 , vol. 29, p. 121
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
参考文献
Seyferth,D. et al.
Journal of Organometallic Chemistry, 1970 , vol. 24, p. 647 - 661
反应条件
methanol; methanol-d1; sodium methylate T=25°C; determination of isotope effect; Rate constantProduct distribution;
参考文献
Eaborn, Colin; Stanczyk, Wlodzimierz A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 4 p. 471 - 473
反应条件
(i) Mg, THF, (ii) /BRN= 1733860/; Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 24, p. 647 - 661
反应条件
(i) nBuLi, hexane, THF, Et2O, pentane, (MeO)2CH2, (ii) /BRN= 1209232/, pentane; Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 24, p. 647 - 661
反应条件
chromium dichloride in tetrahydrofuran T=25°C; 16 h;
参考文献
Takai, Kazuhiko; Kataoka, Yasutaka; Okazoe, Takashi; Utimoto, Kiitiro
Tetrahedron Letters, 1987 , vol. 28, # 13 p. 1443 - 1446