N,N-二甲基-3-苯基-2-丙炔-1-胺合成路线 （共 26 条）
参考文献
Mannich; Chang
Chemische Berichte, 1933 , vol. 66, p. 418
参考文献
Mannich; Chang
Chemische Berichte, 1933 , vol. 66, p. 418
反应条件
ethanol; palladium Hydrogenation;
参考文献
Kruglikova,R.I.; Kalinina,G.R.
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, p. 894 - 897,910 - 912
反应条件
tert.-butylhydroperoxide; copper dichloride in dimethyl sulfoxide
T=20°C; 3 h;
参考文献
Shen, Qi; Zhang, Lei; Zhou, Yu-Ren; Li, Jian-Xin
Tetrahedron Letters, 2013 , vol. 54, # 49 p. 6725 - 6728
反应条件
copper(l) iodide in 1,4-dioxane; water
4 h; Heating;
参考文献
Consorti, Crestina S.; Zanini, Mara L.; Leal, Sheila; Ebeling, Gunter; Dupont, Jairton
Organic Letters, 2003 , vol. 5, # 7 p. 983 - 986
反应条件
potassium hydrogencarbonate; copper(l) iodide in water; dimethyl sulfoxide
T=30°C; 10 h;
参考文献
Bieber, Lothar W.; Da Silva, Margarete F.
Tetrahedron Letters, 2004 , vol. 45, # 45 p. 8281 - 8283
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; N,N-dimethyl-formamide
T=20°C; Alkylation; cross-coupling;
参考文献
Dabdoub, Miguel J.; Dabdoub, Vania B.; Marino, Joseph P.
Tetrahedron Letters, 2000 , vol. 41, # 4 p. 437 - 440
反应条件
copper acetylacetonate in ethylene glycol dimethyl ether
T=110°C; 4 h; Inert atmosphere;
参考文献
Xu, Zhanwei; Yu, Xiaoqiang; Feng, Xiujuan; Bao, Ming
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6901 - 6905
反应条件
N-bromosuccinmide; CuCl2·2H2O; sodium hydrogencarbonate in toluene
T=20 - 110°C; 6 h; Inert atmosphere; Reagent/catalystSolvent;
参考文献
Zhu, Yefeng; Zhao, Huishuang; Wei, Yunyang
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2012-H0052-OP, p. 952 - 958
反应条件
tert.-butylnitrite; trifuran-2-yl-phosphane; palladium diacetate; acetic acid in dimethyl sulfoxide
T=20 - 32°C; Sonogashira coupling; 16 h; Inert atmosphere;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Chemical Communications, 2011 , vol. 47, # 28 p. 7959 - 7961
