N,O-双(三甲基硅烷基)三氟乙酰胺合成路线 (共 118 条)
反应条件
1: o-toluidine With water
T=20°C; UV-irradiation;
2: N,O-bis(trimethylsilyl) trifluoroacetamide With pyridine
T=20°C;
参考文献
An, Taicheng; Sun, Lei; Li, Guiying; Wan, Shungang
Journal of Molecular Catalysis A: Chemical, 2010 , vol. 333, # 1-2 p. 128 - 135
反应条件
pyridine
T=70°C; 1 h;
参考文献
Kotowska, Urszula; Isidorov, Valery A.
Central European Journal of Chemistry, 2011 , vol. 9, # 5 p. 813 - 824
参考文献
Wada, Takeshi; Mochizuki, Akira; Sato, Yuichi; Sekine, Mitsuo
Tetrahedron Letters, 1998 , vol. 39, # 39 p. 7123 - 7126
反应条件
in hexane; dichloromethane
T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
pyridine
T=70°C; 1 h;
参考文献
Kotowska, Urszula; Isidorov, Valery A.
Central European Journal of Chemistry, 2011 , vol. 9, # 5 p. 813 - 824
反应条件
in hexane; dichloromethane
T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: 4-methyl-benzoic acid With cytochrome P450 enzyme CYP199A4 from Rhodopseudomonas palustris HaA2; nicotinamide adenine dinucleotide; bovine liver catalase in ethanol
pH=7.4; Enzymatic reaction;
2: N,O-bis(trimethylsilyl) trifluoroacetamide With chloro-trimethyl-silane in acetonitrile
2 h;
参考文献
Bell, Stephen G.; Zhou, Ruimin; Yang, Wen; Tan, Adrian B. H.; Gentleman, Alexander S.; Wong, Luet-Lok; Zhou, Weihong
Chemistry - A European Journal, 2012 , vol. 18, # 52 p. 16677 - 16688
反应条件
T=125°C; 0.166667 h;
参考文献
Ohashi, Hideo; Yamamoto, Etsuo; Lewis, Norman G.; Towers, G. H. Neil
Phytochemistry (Elsevier), 1987 , vol. 26, # 7 p. 1915 - 1916