7-羟基-4-苯基香豆素合成路线 （共 40 条）
反应条件
silica gel Pechmann condensation; 0.0333333 h; Microwave irradiation;
参考文献
Kuarm, B. Suresh; Madhav, J. Venu; Laxmi, S. Vijaya; Rajitha; Reddy, Y. Thirupathi; Reddy, P. Narsimha; Crooks, Peter A.
Synthetic Communications, 2010 , vol. 40, # 22 p. 3358 - 3364
反应条件
hydrogenchloride 6 h; Reflux;
参考文献
Huazhong University of Science and Technology; NHWA Pharma. Corporation; ZHANG, Guisen; CHEN, Yin; XU, Xiangqing; LIU, Bifeng; LIU, Xin; ZHAO, Song; LIU, Shicheng; YU, Minquan; ZHANG, Heng; LIU, Xinghua
Patent: EP2698369 A1, 2014 ;
Location in patent: Paragraph 0025; 0071 ;
反应条件
5-Nitro-1,10-phenanthroline; oxygen; palladium diacetate in N,N-dimethyl-formamide T=80°C; Heck reaction; 24 h; chemoselective reaction;
参考文献
Li, Yaming; Qi, Zisong; Wang, Huifeng; Fu, Xinmei; Duan, Chunying
Journal of Organic Chemistry, 2012 , vol. 77, # 4 p. 2053 - 2057
反应条件
aminosulfonic acid T=130°C; Pechmann reaction; 0.75 h;
参考文献
Singh, Pankajkumar R.; Singh, Devendrapratap U.; Samant, Shriniwas D.
Synlett, 2004 , # 11 p. 1909 - 1912
反应条件
sulfuric acid in ethyl acetate T=20°C; 12 h;
参考文献
Chemical Communications, , # 31 p. 3296 - 3298
反应条件
polystyrene supported GaCl3 in ethanol 1.41667 h; RefluxGreen chemistry;
参考文献
Rahmatpour, Ali; Mohammadian, Sara
Comptes Rendus Chimie, 2013 , vol. 16, # 3 p. 271 - 278
反应条件
zinc(II) chloride T=100°C; 12 h; neat (no solvent); regioselective reaction;
参考文献
Leao, Raquel A. C.; Def.demoraes, Paula; Pedro, Marcella C. B. C.; Costa, Paulo R. R.
Synthesis, 2011 , # 22 art. no. M70011SS, p. 3692 - 3696
反应条件
PPA; Tl(Oac)3 1 h; Heating;
参考文献
Shamsuddin; Siddiqui, Mohammad Jamshed Ahmed
Journal of Chemical Research - Part S, 1998 , # 7 p. 392 - 393
反应条件
Pd(OPiv)2; silver pivalate; CsO2CCMe3 T=100°C; Inert atmosphere; regioselective reaction;
参考文献
Min, Minsik; Hong, Sungwoo
Chemical Communications, 2012 , vol. 48, # 77 p. 9613 - 9615
